phenyl methanesulfonyl carbamic acid ethylester

Base Information

Chemical Name:phenyl methanesulfonyl carbamic acid ethylester
CAS No.:46731-59-3
Molecular Formula:C₁₀H₁₃NO₄S
Molecular Weight:243.284
Hs Code.:

Synonyms:phenyl methanesulfonyl carbamic acid ethylester

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Chemical Property of phenyl methanesulfonyl carbamic acid ethylester

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Technology Process of phenyl methanesulfonyl carbamic acid ethylester

There total 3 articles about phenyl methanesulfonyl carbamic acid ethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4563-33-1
phenyl-methanesulfonic acid amide

: 541-41-3
chloroformic acid ethyl ester

: 46731-59-3
phenyl methanesulfonyl carbamic acid ethylester

Guidance literature:

Reference yield:

: 100-44-7
benzyl chloride

: 46731-59-3
phenyl methanesulfonyl carbamic acid ethylester

Guidance literature:: Multi-step reaction with 3 steps

1.1: thiourea / ethanol / 1 h / Reflux

1.2: 0.5 h

2.1: ammonia / acetone / 4 h / 0 °C

3.1: potassium carbonate / 4 h / Reflux

With ammonia; potassium carbonate; thiourea; In ethanol; acetone;
DOI:10.1016/j.bmc.2019.05.007

Reference yield:

: 1939-99-7
benzenesulfonyl chloride

: 46731-59-3
phenyl methanesulfonyl carbamic acid ethylester

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia / acetone / 4 h / 0 °C

2: potassium carbonate / 4 h / Reflux

With ammonia; potassium carbonate; In acetone;
DOI:10.1016/j.bmc.2019.05.007