ethyl (-)-(3R)-3-[(3-{[(tert-butoxy)carbonyl]amino}propyl)tosylamino]decanoate

Base Information

Chemical Name:ethyl (-)-(3R)-3-[(3-{[(tert-butoxy)carbonyl]amino}propyl)tosylamino]decanoate
CAS No.:467218-10-6
Molecular Formula:C₂₇H₄₆N₂O₆S
Molecular Weight:526.738
Hs Code.:

Synonyms:ethyl (-)-(3R)-3-[(3-{[(tert-butoxy)carbonyl]amino}propyl)tosylamino]decanoate

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Chemical Property of ethyl (-)-(3R)-3-[(3-{[(tert-butoxy)carbonyl]amino}propyl)tosylamino]decanoate

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Technology Process of ethyl (-)-(3R)-3-[(3-{[(tert-butoxy)carbonyl]amino}propyl)tosylamino]decanoate

There total 8 articles about ethyl (-)-(3R)-3-[(3-{[(tert-butoxy)carbonyl]amino}propyl)tosylamino]decanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 167479-01-8
tert-butyl (3-iodopropyl)carbamate

: 467218-11-7
ethyl (+)-(3R)-3-(tosylamino)decanoate

: 467218-10-6
ethyl (-)-(3R)-3-[(3-{[(tert-butoxy)carbonyl]amino}propyl)tosylamino]decanoate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 55 ℃;
DOI:10.1002/1522-2675(200206)85:6<1659::AID-HLCA1659>3.0.CO;2-D

Reference yield:

: 58885-58-8
N-tert-butoxycarbonyl-3-aminopropanol

: 467218-10-6
ethyl (-)-(3R)-3-[(3-{[(tert-butoxy)carbonyl]amino}propyl)tosylamino]decanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / I₂; 1H-imidazole; PPh₃ / CH₂Cl₂ / 3.5 h / 20 °C

2: 69 percent / Cs₂CO₃ / dimethylformamide / 55 °C

With 1H-imidazole; iodine; caesium carbonate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/1522-2675(200206)85:6<1659::AID-HLCA1659>3.0.CO;2-D

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 467218-10-6
ethyl (-)-(3R)-3-[(3-{[(tert-butoxy)carbonyl]amino}propyl)tosylamino]decanoate

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / Heating

2: 84 percent / I₂; 1H-imidazole; PPh₃ / CH₂Cl₂ / 3.5 h / 20 °C

3: 69 percent / Cs₂CO₃ / dimethylformamide / 55 °C

With 1H-imidazole; iodine; caesium carbonate; triethylamine; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/1522-2675(200206)85:6<1659::AID-HLCA1659>3.0.CO;2-D