allyl 2-O-acetyl-3,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Base Information

Chemical Name:allyl 2-O-acetyl-3,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate
CAS No.:224622-44-0
Molecular Formula:C₂₄H₂₂Cl₃NO₈
Molecular Weight:558.8
Hs Code.:

Synonyms:allyl 2-O-acetyl-3,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 2-O-acetyl-3,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

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Technology Process of allyl 2-O-acetyl-3,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

There total 5 articles about allyl 2-O-acetyl-3,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 545-06-2
trichloroacetonitrile

: 3,4-di-O-benzoyl-2-O-acetyl-α,β-L-rhamnopyranose

: 224622-44-0
allyl 2-O-acetyl-3,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1080/07328309908543994

Reference yield:

: 73-34-7
L-rhamnose

: 224622-44-0
allyl 2-O-acetyl-3,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; sodium acetate / PdCl₂

2: 507 mg / DBU / CH₂Cl₂ / 3 h / 0 °C

With sodium acetate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dichloride; In dichloromethane;
DOI:10.1081/SCC-120027292

Reference yield:

: 98-88-4
benzoyl chloride

: 224622-44-0
allyl 2-O-acetyl-3,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; sodium acetate / PdCl₂

2: 507 mg / DBU / CH₂Cl₂ / 3 h / 0 °C

With sodium acetate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dichloride; In dichloromethane;
DOI:10.1081/SCC-120027292