bis(N(6)-adenosyl)dodecane

Base Information

• Chemical Name: bis(N(6)-adenosyl)dodecane
• CAS No.: 111863-65-1
• Molecular Formula: C32H48 N10 O8
• Molecular Weight: 700.795
• Mol file: 111863-65-1.mol

Synonyms:bis(N(6)-adenosyl)dodecane

Chemical Property of bis(N(6)-adenosyl)dodecane

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 1029.9°Cat760mmHg
• PKA: 12.82±0.70(Predicted)
• Flash Point: 576.7°C
• PSA: 251.10000
• Density: 1.62g/cm³
• LogP: 0.76000

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of bis(N(6)-adenosyl)dodecane

There total 1 articles about bis(N(6)-adenosyl)dodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-phthalimido-1-hexanol (63945-11-9) → N,N''-1,12-dodecanediylbis-Adenosine (111863-65-1)

Guidance literature:

Multi-step reaction with 6 steps

1: 74.4 percent / CBr₄/PPh₃ / acetonitrile / 1 h / Ambient temperature

2: 90.6 percent / toluene / 15 h / Heating

3: 1) t-BuOK / 1) -78 deg C, THF, 2a) -78 deg C, 7h, 2b) -78 deg C to RT, overnight

4: 39 percent / hydrazine hydrate / ethanol

5: 20 percent / pyridine / dimethylaminopyridine / Ambient temperature

6: 64 percent / methanolic ammonia

With pyridine; carbon tetrabromide; potassium tert-butylate; ammonia; hydrazine hydrate; triphenylphosphine; dmap; In ethanol; toluene; acetonitrile;

DOI:10.1016/S0040-4020(01)89771-4

upstream raw materials:

6-phthalimido-1-hexanol

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