(E)-1-(diphenylthiophosphoryl)-3-(1,4-oxazinan-4-ium-4-ylidene)-1,3-diphenyl-1-propene-2-thiolate

Base Information

Chemical Name:(E)-1-(diphenylthiophosphoryl)-3-(1,4-oxazinan-4-ium-4-ylidene)-1,3-diphenyl-1-propene-2-thiolate
CAS No.:602331-15-7
Molecular Formula:C₃₁H₂₈NOPS₂
Molecular Weight:525.675
Hs Code.:

Synonyms:(E)-1-(diphenylthiophosphoryl)-3-(1,4-oxazinan-4-ium-4-ylidene)-1,3-diphenyl-1-propene-2-thiolate

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Chemical Property of (E)-1-(diphenylthiophosphoryl)-3-(1,4-oxazinan-4-ium-4-ylidene)-1,3-diphenyl-1-propene-2-thiolate

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Technology Process of (E)-1-(diphenylthiophosphoryl)-3-(1,4-oxazinan-4-ium-4-ylidene)-1,3-diphenyl-1-propene-2-thiolate

There total 3 articles about (E)-1-(diphenylthiophosphoryl)-3-(1,4-oxazinan-4-ium-4-ylidene)-1,3-diphenyl-1-propene-2-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 602331-03-3
(3-morpholino-1,3-diphenyl-1,2-propadienyl)diphenylphosphane

: 602331-15-7
(E)-1-(diphenylthiophosphoryl)-3-(1,4-oxazinan-4-ium-4-ylidene)-1,3-diphenyl-1-propene-2-thiolate

Guidance literature:: With sulfur; In dichloromethane; for 2h;
DOI:10.1002/ejoc.200300080

Reference yield:

: 115018-09-2
4-(1,3-Diphenyl-2-propinyliden)morpholinium-trifluormethansulfonat

: 602331-15-7
(E)-1-(diphenylthiophosphoryl)-3-(1,4-oxazinan-4-ium-4-ylidene)-1,3-diphenyl-1-propene-2-thiolate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / LiCl / tetrahydrofuran / -78 - 20 °C

2: 91 percent / sulfur / CH₂Cl₂ / 2 h

With sulfur; lithium chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.200300080

Reference yield:

: 17154-34-6
(trimethylsilyl)diphenylphosphine

: 602331-15-7
(E)-1-(diphenylthiophosphoryl)-3-(1,4-oxazinan-4-ium-4-ylidene)-1,3-diphenyl-1-propene-2-thiolate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / LiCl / tetrahydrofuran / -78 - 20 °C

2: 91 percent / sulfur / CH₂Cl₂ / 2 h

With sulfur; lithium chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.200300080