(3R)-5-(benzyloxy)-3-methylpentanal

Base Information

Chemical Name:(3R)-5-(benzyloxy)-3-methylpentanal
CAS No.:82538-58-7
Molecular Formula:C₁₃H₁₈O₂
Molecular Weight:206.285
Hs Code.:

Synonyms:(3R)-5-(benzyloxy)-3-methylpentanal

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Chemical Property of (3R)-5-(benzyloxy)-3-methylpentanal

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Technology Process of (3R)-5-(benzyloxy)-3-methylpentanal

There total 14 articles about (3R)-5-(benzyloxy)-3-methylpentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 161905-08-4
(S,E)-8-(benzyloxy)-2,6-dimethyl-3-octen-2-ol

: 82538-58-7
(3R)-5-(benzyloxy)-3-methylpentanal

Guidance literature:: (S,E)-8-(benzyloxy)-2,6-dimethyl-3-octen-2-ol; With ozone; In methanol; at -50 ℃;

With dimethylsulfide; In methanol; at -60 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.11.054

Reference yield: 66.0%

: 100-44-7
benzyl chloride

: (3R)-3-methyl-5-(tetrahydro-2H-pyran-2-yloxy)-pentan-1-ol

: 82538-58-7
(3R)-5-(benzyloxy)-3-methylpentanal

Guidance literature:: (3R)-3-methyl-5-(tetrahydro-2H-pyran-2-yloxy)-pentan-1-ol; With sodium hydride; In tetrahydrofuran; for 0.333333h;

benzyl chloride; In tetrahydrofuran; at 50 ℃; for 8h; Further stages;
DOI:10.1134/S1070428015030094

Reference yield:

: (4R)-4-phenyl-3-[(3S)-3-methylhex-5-enoyl]oxazolidin-2-one

: 82538-58-7
(3R)-5-(benzyloxy)-3-methylpentanal

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / tetrahydrofuran; water / 4 h / 0 - 20 °C / Inert atmosphere

2: sodium hydride / tetrahydrofuran; water; mineral oil / 2.5 h / 0 - 20 °C / Inert atmosphere

3: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 4 h / 20 °C / Inert atmosphere

4: sodium periodate / water; formic acid / 1 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; sodium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; formic acid; water; acetone; mineral oil;
DOI:10.1002/asia.201402593