Toluene-4-sulfonic acid (R)-1-(2-benzenesulfonyl-ethyl)-4-methyl-pentyl ester

Base Information

Chemical Name:Toluene-4-sulfonic acid (R)-1-(2-benzenesulfonyl-ethyl)-4-methyl-pentyl ester
CAS No.:195988-94-4
Molecular Formula:C₂₁H₂₈O₅S₂
Molecular Weight:424.582
Hs Code.:

Synonyms:Toluene-4-sulfonic acid (R)-1-(2-benzenesulfonyl-ethyl)-4-methyl-pentyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Toluene-4-sulfonic acid (R)-1-(2-benzenesulfonyl-ethyl)-4-methyl-pentyl ester

Chemical Property:

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Technology Process of Toluene-4-sulfonic acid (R)-1-(2-benzenesulfonyl-ethyl)-4-methyl-pentyl ester

There total 6 articles about Toluene-4-sulfonic acid (R)-1-(2-benzenesulfonyl-ethyl)-4-methyl-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 13438-45-4
zinc(II) tosylate

: 195988-81-9
(S)-1-Benzenesulfonyl-6-methyl-heptan-3-ol

: 195988-94-4
Toluene-4-sulfonic acid (R)-1-(2-benzenesulfonyl-ethyl)-4-methyl-pentyl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In benzene; 1.) 50 deg C, 30 min, 2.) 35 deg C, 10 h;

Reference yield:

: 61955-91-7
1-chloro-4-(phenylthio)butan-2-one

: 195988-94-4
Toluene-4-sulfonic acid (R)-1-(2-benzenesulfonyl-ethyl)-4-methyl-pentyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 30percent aq. H₂O₂, Na₂WO₄*2H₂O / methanol / 10 h / Ambient temperature

2: sucrose, Bakers' yeast / H₂O / 120 h / 30 °C

3: 95 percent / NaOH / methanol / 1.) 0 deg C, 30 min, 2.) r.t., 2 h

4: 1.) Mg, 2.) CuI / 1.) THF, r.t., 2.) THF, 0 deg C, 2 h

5: 79 percent / DEAD, Ph₃P / benzene / 1.) 50 deg C, 30 min, 2.) 35 deg C, 10 h

With sodium hydroxide; sodium tungstate; copper(l) iodide; bakers' yeast; dihydrogen peroxide; magnesium; triphenylphosphine; Sucrose; diethylazodicarboxylate; In methanol; water; benzene;

Reference yield:

: 108-98-5
thiophenol

: 195988-94-4
Toluene-4-sulfonic acid (R)-1-(2-benzenesulfonyl-ethyl)-4-methyl-pentyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: Et₃N / benzene / 10 h / Ambient temperature

2: 30percent aq. H₂O₂, Na₂WO₄*2H₂O / methanol / 10 h / Ambient temperature

3: sucrose, Bakers' yeast / H₂O / 120 h / 30 °C

4: 95 percent / NaOH / methanol / 1.) 0 deg C, 30 min, 2.) r.t., 2 h

5: 1.) Mg, 2.) CuI / 1.) THF, r.t., 2.) THF, 0 deg C, 2 h

6: 79 percent / DEAD, Ph₃P / benzene / 1.) 50 deg C, 30 min, 2.) 35 deg C, 10 h

With sodium hydroxide; sodium tungstate; copper(l) iodide; bakers' yeast; dihydrogen peroxide; magnesium; triethylamine; triphenylphosphine; Sucrose; diethylazodicarboxylate; In methanol; water; benzene;