6aα-<2-(benzyloxy)ethyl>-9aα-<2-(trimethylacetamido)phenyl>-1,2,4,6a,7,8,9,9bα-octahydro-9H-pyrrolo<3,2,1-ij>quinolin-9-one

Base Information

Chemical Name:6aα-<2-(benzyloxy)ethyl>-9aα-<2-(trimethylacetamido)phenyl>-1,2,4,6a,7,8,9,9bα-octahydro-9H-pyrrolo<3,2,1-ij>quinolin-9-one
CAS No.:119146-66-6
Molecular Formula:C₃₁H₃₈N₂O₃
Molecular Weight:486.654
Hs Code.:

Synonyms:6aα-<2-(benzyloxy)ethyl>-9aα-<2-(trimethylacetamido)phenyl>-1,2,4,6a,7,8,9,9bα-octahydro-9H-pyrrolo<3,2,1-ij>quinolin-9-one

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Chemical Property of 6aα-<2-(benzyloxy)ethyl>-9aα-<2-(trimethylacetamido)phenyl>-1,2,4,6a,7,8,9,9bα-octahydro-9H-pyrrolo<3,2,1-ij>quinolin-9-one

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Technology Process of 6aα-<2-(benzyloxy)ethyl>-9aα-<2-(trimethylacetamido)phenyl>-1,2,4,6a,7,8,9,9bα-octahydro-9H-pyrrolo<3,2,1-ij>quinolin-9-one

There total 21 articles about 6aα-<2-(benzyloxy)ethyl>-9aα-<2-(trimethylacetamido)phenyl>-1,2,4,6a,7,8,9,9bα-octahydro-9H-pyrrolo<3,2,1-ij>quinolin-9-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 119146-65-5
4aα-<2-(benzyloxy)ethyl>-7a-<1-<2-(trimethylacetamido)phenyl>ethenyl>-2,4a,5,6,7,7aα-hexahydro-1H-1-pyridin-7-ol

: 119146-66-6
6aα-<2-(benzyloxy)ethyl>-9aα-<2-(trimethylacetamido)phenyl>-1,2,4,6a,7,8,9,9bα-octahydro-9H-pyrrolo<3,2,1-ij>quinolin-9-one

Guidance literature:: With camphor-10-sulfonic acid; In benzene; for 3h; Heating;

Reference yield:

: 97552-28-8
2-<2-(trimethylacetamido)phenyl>-2-<(trimethylsilyl)oxy>acetonitrile

: 119146-66-6
6aα-<2-(benzyloxy)ethyl>-9aα-<2-(trimethylacetamido)phenyl>-1,2,4,6a,7,8,9,9bα-octahydro-9H-pyrrolo<3,2,1-ij>quinolin-9-one

Guidance literature:: Multi-step reaction with 3 steps

2: 1.) Ph₃P=CH₂, 2.) KOH / 1.) 23 deg C, 2.) EtOH/H₂O, 130 deg C

3: 82 percent / camphorsulfonic acid / benzene / 3 h / Heating

With potassium hydroxide; camphor-10-sulfonic acid; Methylenetriphenylphosphorane; In benzene;
DOI:10.1021/jo00267a003

Reference yield:

: 119146-63-3
4aα-<2-(benzyloxy)ethyl>-1-(methoxycarbonyl)-1,2,4a,5,6,7aα-hexahydro-7H-1-pyrindin-7-one

: 119146-66-6
6aα-<2-(benzyloxy)ethyl>-9aα-<2-(trimethylacetamido)phenyl>-1,2,4,6a,7,8,9,9bα-octahydro-9H-pyrrolo<3,2,1-ij>quinolin-9-one

Guidance literature:: Multi-step reaction with 3 steps

2: 1.) Ph₃P=CH₂, 2.) KOH / 1.) 23 deg C, 2.) EtOH/H₂O, 130 deg C

3: 82 percent / camphorsulfonic acid / benzene / 3 h / Heating

With potassium hydroxide; camphor-10-sulfonic acid; Methylenetriphenylphosphorane; In benzene;
DOI:10.1021/jo00267a003