C₁₄H₁₂FN₅O₃

Base Information

Chemical Name:C₁₄H₁₂FN₅O₃
CAS No.:1338091-04-5
Molecular Formula:C₁₄H₁₂FN₅O₃
Molecular Weight:317.279
Hs Code.:

C<sub>14</sub>H<sub>12</sub>FN<sub>5</sub>O<sub>3</sub>

Synonyms:C₁₄H₁₂FN₅O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₂FN₅O₃

Chemical Property:

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Technology Process of C₁₄H₁₂FN₅O₃

There total 13 articles about C₁₄H₁₂FN₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1338091-29-4
5-benzyloxy-6-[5-(4-fluorobenzyl)[1,3,4]oxadiazol-2-yl]-3-methyl-3H-pyrimidin-4-one oxime

: 1338091-04-5
C₁₄H₁₂FN₅O₃

Guidance literature:: With hydrogen; palladium 10% on activated carbon; at 20 ℃; under 760.051 Torr; Product distribution / selectivity;

Reference yield:

: 405-50-5
p-Fluorophenylacetic acid

: 1338091-04-5
C₁₄H₁₂FN₅O₃

Guidance literature:: Multi-step reaction with 7 steps

1: thionyl chloride / 1 h / 80 °C

2: hydrazine hydrate / dichloromethane / 1.5 h / 0 - 20 °C

3: triethylamine / dichloromethane / 0 - 20 °C

4: triphenylphosphine; tetrachloromethane / acetonitrile / 20 °C

5: Lawessons reagent / toluene / 14 h / 80 - 85 °C

6: mercury(II) diacetate; N,O-bis(trimethylsilyl)hydroxylamine / 1,4-dioxane / 1 h / 20 °C

7: hydrogen / palladium 10% on activated carbon / 20 °C / 760.05 Torr

With Lawessons reagent; tetrachloromethane; thionyl chloride; N,O-bis(trimethylsilyl)hydroxylamine; mercury(II) diacetate; hydrogen; hydrazine hydrate; triethylamine; triphenylphosphine; palladium 10% on activated carbon; In 1,4-dioxane; dichloromethane; toluene; acetonitrile;

Reference yield:

: 459-04-1
4-Fluorophenylacetyl chloride

: 1338091-04-5
C₁₄H₁₂FN₅O₃

Guidance literature:: Multi-step reaction with 6 steps

1: hydrazine hydrate / dichloromethane / 1.5 h / 0 - 20 °C

2: triethylamine / dichloromethane / 0 - 20 °C

3: triphenylphosphine; tetrachloromethane / acetonitrile / 20 °C

4: Lawessons reagent / toluene / 14 h / 80 - 85 °C

5: mercury(II) diacetate; N,O-bis(trimethylsilyl)hydroxylamine / 1,4-dioxane / 1 h / 20 °C

6: hydrogen / palladium 10% on activated carbon / 20 °C / 760.05 Torr

With Lawessons reagent; tetrachloromethane; N,O-bis(trimethylsilyl)hydroxylamine; mercury(II) diacetate; hydrogen; hydrazine hydrate; triethylamine; triphenylphosphine; palladium 10% on activated carbon; In 1,4-dioxane; dichloromethane; toluene; acetonitrile;