2,6-Dichloro-α-(4-chlorophenyl)-4-nitrobenzeneacetonitrile

Base Information

Chemical Name:2,6-Dichloro-α-(4-chlorophenyl)-4-nitrobenzeneacetonitrile
CAS No.:103317-59-5
Molecular Formula:C₁₄H₇Cl₃N₂O₂
Molecular Weight:341.581
Hs Code.:
Mol file:103317-59-5.mol

Synonyms:2-(4'-chlorophenyl)-2-(2,6-dichloro-4-nitrophenyl)acetonitrile

Suppliers and Price of 2,6-Dichloro-α-(4-chlorophenyl)-4-nitrobenzeneacetonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,?6-?Dichloro-?α-?(4-?chlorophenyl)?-?4-?nitrobenzeneacetonitrile
10g
$ 425.00

Medical Isotopes, Inc.
2,6-Dichloro-α-(4-chlorophenyl)-4-nitrobenzeneacetonitrile
50 g
$ 2275.00

Medical Isotopes, Inc.
2,6-Dichloro-α-(4-chlorophenyl)-4-nitrobenzeneacetonitrile
10 g
$ 925.00

Total 2 raw suppliers

Chemical Property of 2,6-Dichloro-α-(4-chlorophenyl)-4-nitrobenzeneacetonitrile

Chemical Property:

Melting Point:106 - 112oC
Storage Temp.:Refrigerator
Solubility.:Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)

Purity/Quality:: 2,?6-?Dichloro-?α-?(4-?chlorophenyl)?-?4-?nitrobenzeneacetonitrile ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 2,6-Dichloro-α-(4-chlorophenyl)-4-nitrobenzeneacetonitrile is used in the synthesis of anticoccidial triazine compounds.

Technology Process of 2,6-Dichloro-α-(4-chlorophenyl)-4-nitrobenzeneacetonitrile

There total 3 articles about 2,6-Dichloro-α-(4-chlorophenyl)-4-nitrobenzeneacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 20098-48-0
3,4,5-trichloronitrobenzen

: 140-53-4
p-chlorobenzyl cyanide

: 103317-59-5
2-(4'-chlorophenyl)-2-(2,6-dichloro-4-nitrophenyl)acetonitrile

Guidance literature:: 3,4,5-trichloronitrobenzen; With tetrabutylammomium bromide; sodium hydroxide; In water; for 0.5h;

p-chlorobenzyl cyanide; In tetrahydrofuran; water; at 60 ℃; for 8h;

Reference yield:

: 20098-48-0
3,4,5-trichloronitrobenzen

: 56-37-1
N-benzyl-N,N,N-triethylammonium chloride

: 140-53-4
p-chlorobenzyl cyanide

: 103317-59-5
2-(4'-chlorophenyl)-2-(2,6-dichloro-4-nitrophenyl)acetonitrile

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; di-isopropyl ether;

Reference yield:

: 99-30-9
4-nitro-2,6-dichloroaniline

: 103317-59-5
2-(4'-chlorophenyl)-2-(2,6-dichloro-4-nitrophenyl)acetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid; sodium nitrite / 0.33 h / 5 - 70 °C

1.2: 0.5 h

1.3: 1 h / 25 - 70 °C

2.1: sodium hydroxide / butanone / 2 h / 50 °C

With sulfuric acid; sodium hydroxide; sodium nitrite; In butanone;