Technology Process of C40H30N4
There total 4 articles about C40H30N4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; sodium carbonate;
In
tetrahydrofuran; water;
at 65 ℃;
for 12h;
Inert atmosphere;
DOI:10.1039/c4ob00901k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonium hydroxide / 1.5 h / 60 °C
2: trifluoroacetic anhydride; pyridine / 1,4-dioxane / 12 h / 0 - 25 °C
3: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / water; tetrahydrofuran / 12 h / 65 °C / Inert atmosphere
With
pyridine; bis-triphenylphosphine-palladium(II) chloride; ammonium hydroxide; sodium carbonate; trifluoroacetic anhydride;
In
tetrahydrofuran; 1,4-dioxane; water;
3: |Suzuki-Miyaura Coupling;
DOI:10.1039/c4ob00901k
- Guidance literature:
-
Multi-step reaction with 4 steps
1: fuming sulphuric acid; iodine / 24 h / 70 °C
2: ammonium hydroxide / 1.5 h / 60 °C
3: trifluoroacetic anhydride; pyridine / 1,4-dioxane / 12 h / 0 - 25 °C
4: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / water; tetrahydrofuran / 12 h / 65 °C / Inert atmosphere
With
pyridine; bis-triphenylphosphine-palladium(II) chloride; ammonium hydroxide; fuming sulphuric acid; iodine; sodium carbonate; trifluoroacetic anhydride;
In
tetrahydrofuran; 1,4-dioxane; water;
4: |Suzuki-Miyaura Coupling;
DOI:10.1039/c4ob00901k