C₃₃H₆₂O₃SiSn

Base Information

Chemical Name:C₃₃H₆₂O₃SiSn
CAS No.:1395345-63-7
Molecular Formula:C₃₃H₆₂O₃SiSn
Molecular Weight:653.649
Hs Code.:

C<sub>33</sub>H<sub>62</sub>O<sub>3</sub>SiSn

Synonyms:C₃₃H₆₂O₃SiSn

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Chemical Property of C₃₃H₆₂O₃SiSn

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Technology Process of C₃₃H₆₂O₃SiSn

There total 10 articles about C₃₃H₆₂O₃SiSn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1395345-61-5
C₂₁H₃₄O₃Si

: 688-73-3
tri-n-butyl-tin hydride

: 1395345-63-7
C₃₃H₆₂O₃SiSn

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 23 ℃; for 0.5h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c2ob26906f

Reference yield:

: 132969-71-2
methyl (2S)-[(4-methoxybenzyl)oxy]-2-methylpropanoate

: 1395345-63-7
C₃₃H₆₂O₃SiSn

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / dichloromethane / 4.42 h / -78 °C / Inert atmosphere; Schlenk technique

2.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 23 °C / Inert atmosphere; Schlenk technique

3.1: diethylzinc / toluene / 1 h / Inert atmosphere; Schlenk technique; Reflux

3.2: 1 h / 23 °C / Inert atmosphere; Schlenk technique

3.3: Inert atmosphere; Schlenk technique

4.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere; Schlenk technique

5.1: potassium carbonate / methanol / 1 h / 23 °C / Inert atmosphere; Schlenk technique

6.1: n-butyllithium / tetrahydrofuran / 0.08 h / -78 - 0 °C / Inert atmosphere; Schlenk technique

6.2: -78 - 23 °C / Inert atmosphere; Schlenk technique

7.1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0.5 h / 23 °C / Inert atmosphere; Schlenk technique

With 2,6-dimethylpyridine; bis-triphenylphosphine-palladium(II) chloride; n-butyllithium; diethylzinc; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1039/c2ob26906f

Reference yield:

: 136320-64-4
(2R)-3-[(4-methoxybenzyl)oxy]-2-methylpropanol

: 1395345-63-7
C₃₃H₆₂O₃SiSn

Guidance literature:: Multi-step reaction with 6 steps

1.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 23 °C / Inert atmosphere; Schlenk technique

2.1: diethylzinc / toluene / 1 h / Inert atmosphere; Schlenk technique; Reflux

2.2: 1 h / 23 °C / Inert atmosphere; Schlenk technique

2.3: Inert atmosphere; Schlenk technique

3.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere; Schlenk technique

4.1: potassium carbonate / methanol / 1 h / 23 °C / Inert atmosphere; Schlenk technique

5.1: n-butyllithium / tetrahydrofuran / 0.08 h / -78 - 0 °C / Inert atmosphere; Schlenk technique

5.2: -78 - 23 °C / Inert atmosphere; Schlenk technique

6.1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0.5 h / 23 °C / Inert atmosphere; Schlenk technique

With 2,6-dimethylpyridine; bis-triphenylphosphine-palladium(II) chloride; n-butyllithium; diethylzinc; potassium carbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1039/c2ob26906f