(-)-methyl 4-[N-(4-methoxyphenyl)amino]-4-phenylbutanoate

Base Information

Chemical Name:(-)-methyl 4-[N-(4-methoxyphenyl)amino]-4-phenylbutanoate
CAS No.:188488-71-3
Molecular Formula:C₁₈H₂₁NO₃
Molecular Weight:299.37
Hs Code.:

Synonyms:(-)-methyl 4-[N-(4-methoxyphenyl)amino]-4-phenylbutanoate

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Chemical Property of (-)-methyl 4-[N-(4-methoxyphenyl)amino]-4-phenylbutanoate

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Technology Process of (-)-methyl 4-[N-(4-methoxyphenyl)amino]-4-phenylbutanoate

There total 5 articles about (-)-methyl 4-[N-(4-methoxyphenyl)amino]-4-phenylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1357377-74-2
methyl 4-(N-4-methoxyphenylimino)-4-phenylbutanoate

: 1170700-44-3
2-methoxy-1-(4-methoxyphenyl)-5-phenyl-1H-pyrrole

: 188488-71-3
(-)-methyl 4-[N-(4-methoxyphenyl)amino]-4-phenylbutanoate

: 188488-72-4
methyl 4-[N-(4-methoxyphenyl)amino]-4-phenylbutanoate

Guidance literature:: With (S)-(-)-N-(3',5'-di-tert-butylphenyl)-2-[formyl(methyl)amino]-3-methylbutanamide; trichlorosilane; In toluene; at 18 ℃; for 16h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/jo900561h

Reference yield:

: C₂₀H₂₃NO₅

: 188488-71-3
(-)-methyl 4-[N-(4-methoxyphenyl)amino]-4-phenylbutanoate

Guidance literature:: With water; lithium chloride; In dimethyl sulfoxide; at 130 ℃; for 2h;
DOI:10.1021/acscatal.9b02523

Reference yield:

: 104-94-9
4-methoxy-aniline

: 188488-71-3
(-)-methyl 4-[N-(4-methoxyphenyl)amino]-4-phenylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: ytterbium tris<(R)-(-)-1,1'-binaphthyl-2,2'-diyl phosphate>; yttrium(III) trifluoromethanesulfonate / m-xylene; water / 48 h / 0 °C / Molecular sieve

2: lithium chloride; water / dimethyl sulfoxide / 2 h / 130 °C

With ytterbium tris<(R)-(-)-1,1'-binaphthyl-2,2'-diyl phosphate>; water; lithium chloride; yttrium(III) trifluoromethanesulfonate; In water; dimethyl sulfoxide; m-xylene;
DOI:10.1021/acscatal.9b02523