N-Boc-N-(tert-butyloxycarbonylmethylene)-(D)-cyclohexylalanine benzyl ester

Base Information

Chemical Name:N-Boc-N-(tert-butyloxycarbonylmethylene)-(D)-cyclohexylalanine benzyl ester
CAS No.:203789-94-0
Molecular Formula:C₂₇H₄₁NO₆
Molecular Weight:475.626
Hs Code.:

Synonyms:N-Boc-N-(tert-butyloxycarbonylmethylene)-(D)-cyclohexylalanine benzyl ester

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Chemical Property of N-Boc-N-(tert-butyloxycarbonylmethylene)-(D)-cyclohexylalanine benzyl ester

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Technology Process of N-Boc-N-(tert-butyloxycarbonylmethylene)-(D)-cyclohexylalanine benzyl ester

There total 5 articles about N-Boc-N-(tert-butyloxycarbonylmethylene)-(D)-cyclohexylalanine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58717-02-5
3-cyclohexyl-D-alanine

: 203789-94-0
N-Boc-N-(tert-butyloxycarbonylmethylene)-(D)-cyclohexylalanine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / toluene

2: i-Pr₂NEt / dimethylformamide / 20 h

3: i-Pr₂NEt / dimethylformamide / 24 h / 40 °C

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-2004-831200

Reference yield:

: 203789-93-9
N-(tert-butyloxycarbonylmethylene)-(D)-cyclohexylalanine benzyl ester

: 24424-99-5
di-tert-butyl dicarbonate

: 203789-94-0
N-Boc-N-(tert-butyloxycarbonylmethylene)-(D)-cyclohexylalanine benzyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 40 ℃; for 24h;
DOI:10.1055/s-2004-831200

Reference yield:

: benzyl (2R)-2-amino-3-cyclohexylpropanoate 4-methylbenzenesulfonic salt

: 203789-94-0
N-Boc-N-(tert-butyloxycarbonylmethylene)-(D)-cyclohexylalanine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: i-Pr₂NEt / dimethylformamide / 20 h

2: i-Pr₂NEt / dimethylformamide / 24 h / 40 °C

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1055/s-2004-831200