octyl 2,3,4-tri-O-benzyl-6-O-trityl-α-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

Base Information

• Chemical Name: octyl 2,3,4-tri-O-benzyl-6-O-trityl-α-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside
• CAS No.: 172039-01-9
• Molecular Formula: C₈₁H₈₈O₁₁
• Molecular Weight: 1237.58
• Mol file: 172039-01-9.mol

Synonyms:octyl 2,3,4-tri-O-benzyl-6-O-trityl-α-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

Chemical Property of octyl 2,3,4-tri-O-benzyl-6-O-trityl-α-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of octyl 2,3,4-tri-O-benzyl-6-O-trityl-α-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

There total 1 articles about octyl 2,3,4-tri-O-benzyl-6-O-trityl-α-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

benzyl bromide (100-39-0) + octyl 6-O-trityl-α-D-galactopyranosyl-(1->6)-β-D-glucopyranoside → octyl 2,3,4-tri-O-benzyl-6-O-trityl-α-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside (172039-01-9)

Guidance literature:

With potassium hydroxide; In dimethyl sulfoxide; for 48h; Ambient temperature;

DOI:10.1016/0008-6215(95)00108-6

Reference yield: 97.0%

octyl 2,3,4-tri-O-benzyl-6-O-trityl-α-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside (172039-01-9) → octyl 2,3,4-tri-O-benzyl-α-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside (172039-02-0)

Guidance literature:

With chloro-trimethyl-silane; sodium iodide; In acetonitrile; at 0 ℃; for 2h;

DOI:10.1016/0008-6215(95)00108-6

Reference yield:

octyl 2,3,4-tri-O-benzyl-6-O-trityl-α-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside (172039-01-9) → C67H84O11

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / NaI, chlorotrimethylsilane / acetonitrile / 2 h / 0 °C

2: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, 24 h

With chloro-trimethyl-silane; sodium hydride; sodium iodide; In acetonitrile;

DOI:10.1016/0008-6215(95)00108-6

upstream raw materials:

benzyl bromide

Downstream raw materials:

octyl 2,3,4-tri-O-benzyl-α-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside