benzyl(E)-2-benzyloxycarbonyl-3-isopropyl-5-(methylsulfonyloxyimino)hexanoate

Base Information

Chemical Name:benzyl(E)-2-benzyloxycarbonyl-3-isopropyl-5-(methylsulfonyloxyimino)hexanoate
CAS No.:264599-10-2
Molecular Formula:C₂₅H₃₁NO₇S
Molecular Weight:489.59
Hs Code.:

Synonyms:benzyl(E)-2-benzyloxycarbonyl-3-isopropyl-5-(methylsulfonyloxyimino)hexanoate

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Chemical Property of benzyl(E)-2-benzyloxycarbonyl-3-isopropyl-5-(methylsulfonyloxyimino)hexanoate

Chemical Property:

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Technology Process of benzyl(E)-2-benzyloxycarbonyl-3-isopropyl-5-(methylsulfonyloxyimino)hexanoate

There total 4 articles about benzyl(E)-2-benzyloxycarbonyl-3-isopropyl-5-(methylsulfonyloxyimino)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-63-0
methanesulfonyl chloride

: 264599-18-0
benzyl(E)-2-benzyloxycarbonyl-5-hydroxyimino-3-isopropylhexanoate

: 264599-10-2
benzyl(E)-2-benzyloxycarbonyl-3-isopropyl-5-(methylsulfonyloxyimino)hexanoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

: 5166-53-0
5-methyl-3-hexene-2-one

: 264599-10-2
benzyl(E)-2-benzyloxycarbonyl-3-isopropyl-5-(methylsulfonyloxyimino)hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: tert-BuOK / tetrahydrofuran / 4 h / 25 °C

2: H₂NOH*HCl; Na₂CO₃ / H₂O; methanol / 4 h / 25 °C

3: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With hydroxylamine hydrochloride; potassium tert-butylate; sodium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; 1: Addition / 2: Condensation / 3: Acylation;

Reference yield:

: 15014-25-2
malonic acid dibenzyl ester

: 264599-10-2
benzyl(E)-2-benzyloxycarbonyl-3-isopropyl-5-(methylsulfonyloxyimino)hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: tert-BuOK / tetrahydrofuran / 4 h / 25 °C

2: H₂NOH*HCl; Na₂CO₃ / H₂O; methanol / 4 h / 25 °C

3: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With hydroxylamine hydrochloride; potassium tert-butylate; sodium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; 1: Addition / 2: Condensation / 3: Acylation;