C₂₈H₃₃ClFN₅O₅S

Base Information

Chemical Name:C₂₈H₃₃ClFN₅O₅S
CAS No.:1402586-79-1
Molecular Formula:C₂₈H₃₃ClFN₅O₅S
Molecular Weight:606.118
Hs Code.:

C<sub>28</sub>H<sub>33</sub>ClFN<sub>5</sub>O<sub>5</sub>S

Synonyms:C₂₈H₃₃ClFN₅O₅S

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Chemical Property of C₂₈H₃₃ClFN₅O₅S

Chemical Property:

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Technology Process of C₂₈H₃₃ClFN₅O₅S

There total 9 articles about C₂₈H₃₃ClFN₅O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402586-78-0
C₂₃H₂₄ClFN₄O

: 352275-00-4,872496-91-8
(tert-butoxycarbonyl)-((4-(dimethyliminio)pyridin-1(4H)-yl)sulfonyl)amide

: 1402586-79-1
C₂₈H₃₃ClFN₅O₅S

Guidance literature:: With triethylamine; In dichloromethane; at 23 ℃; for 15h;

Reference yield:

: 95037-98-2
ethyl 2-(4-amino-3-fluorophenyl)propionate

: 1402586-79-1
C₂₈H₃₃ClFN₅O₅S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium nitrite; toluene-4-sulfonic acid; potassium iodide / water; acetonitrile / 4.17 h / 10 - 20 °C

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis-(diphenylphosphino)ferrocene; zinc / N,N-dimethyl acetamide / 15 h / 120 °C / Inert atmosphere

3.1: water; sodium hydroxide / tetrahydrofuran / 15 h / 23 °C

4.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / 23 °C

5.1: nickel(II) chloride hexahydrate / ethanol / 0.25 h

5.2: 2 h

6.1: triethylamine / dichloromethane / 15 h / 23 °C

With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; nickel(II) chloride hexahydrate; water; benzotriazol-1-ol; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium iodide; sodium hydroxide; zinc; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl acetamide; water; acetonitrile;

Reference yield:

: 78543-07-4
ethyl 2-(3-fluoro-4-nitrophenyl)propionate

: 1402586-79-1
C₂₈H₃₃ClFN₅O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: palladium 10% on activated carbon; hydrogen / ethanol; tetrahydrofuran / 6 h

2.1: sodium nitrite; toluene-4-sulfonic acid; potassium iodide / water; acetonitrile / 4.17 h / 10 - 20 °C

3.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis-(diphenylphosphino)ferrocene; zinc / N,N-dimethyl acetamide / 15 h / 120 °C / Inert atmosphere

4.1: water; sodium hydroxide / tetrahydrofuran / 15 h / 23 °C

5.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / 23 °C

6.1: nickel(II) chloride hexahydrate / ethanol / 0.25 h

6.2: 2 h

7.1: triethylamine / dichloromethane / 15 h / 23 °C

With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; nickel(II) chloride hexahydrate; palladium 10% on activated carbon; water; hydrogen; benzotriazol-1-ol; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium iodide; sodium hydroxide; zinc; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl acetamide; water; acetonitrile;