C₅₀H₆₆N₄O₁₂

Base Information

Chemical Name:C₅₀H₆₆N₄O₁₂
CAS No.:1419388-22-9
Molecular Formula:C₅₀H₆₆N₄O₁₂
Molecular Weight:915.094
Hs Code.:

C<sub>50</sub>H<sub>66</sub>N<sub>4</sub>O<sub>12</sub>

Synonyms:C₅₀H₆₆N₄O₁₂

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Chemical Property of C₅₀H₆₆N₄O₁₂

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Technology Process of C₅₀H₆₆N₄O₁₂

There total 9 articles about C₅₀H₆₆N₄O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1318898-55-3
N-[(methyloxy)carbonyl]-L-valyl-(4S)-4-methyl-L-proline

: 1419392-29-2
C₂₄H₂₄Br₂O₂

: 1419388-22-9
C₅₀H₆₆N₄O₁₂

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 3h;

Reference yield:

: 98-79-3
L-Pyroglutamic acid

: 1419388-22-9
C₅₀H₆₆N₄O₁₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: thionyl chloride / 3.5 h / 0 - 20 °C

2.1: dmap / acetonitrile / 18 h / 20 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C

3.2: -78 - 20 °C

4.1: borane-THF / tetrahydrofuran / 10 h / 40 °C

5.1: hydrogenchloride / ethyl acetate / 20 °C / Cooling with ice

6.1: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

7.1: lithium hydroxide / tetrahydrofuran; water / 0 - 20 °C

8.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 0.08 h

8.2: 3 h / 20 °C

With hydrogenchloride; dmap; thionyl chloride; borane-THF; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; lithium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; ethyl acetate; acetonitrile;

Reference yield:

: 7149-65-7
ethyl (S)-pyroglutamate

: 1419388-22-9
C₅₀H₆₆N₄O₁₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: dmap / acetonitrile / 18 h / 20 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C

2.2: -78 - 20 °C

3.1: borane-THF / tetrahydrofuran / 10 h / 40 °C

4.1: hydrogenchloride / ethyl acetate / 20 °C / Cooling with ice

5.1: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

6.1: lithium hydroxide / tetrahydrofuran; water / 0 - 20 °C

7.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 0.08 h

7.2: 3 h / 20 °C

With hydrogenchloride; dmap; borane-THF; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; lithium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; ethyl acetate; acetonitrile;