η6-[1-(2-methylphenyl)-4-methoxybenzene]tricarbonylchromium(0)

Base Information

Chemical Name:η6-[1-(2-methylphenyl)-4-methoxybenzene]tricarbonylchromium(0)
CAS No.:324745-58-6
Molecular Formula:C₁₇H₁₄CrO₄
Molecular Weight:334.292
Hs Code.:

Synonyms:η6-[1-(2-methylphenyl)-4-methoxybenzene]tricarbonylchromium(0)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of η6-[1-(2-methylphenyl)-4-methoxybenzene]tricarbonylchromium(0)

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Technology Process of η6-[1-(2-methylphenyl)-4-methoxybenzene]tricarbonylchromium(0)

There total 1 articles about η6-[1-(2-methylphenyl)-4-methoxybenzene]tricarbonylchromium(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 56213-59-3
η6-(4-methoxyfluorobenzene)tricarbonylchromium(0)

: 16419-60-6
2-Methylphenylboronic acid

: 324745-58-6
η6-[1-(2-methylphenyl)-4-methoxybenzene]tricarbonylchromium(0)

Guidance literature:: With caesium carbonate; trimethylphosphane; In 1,2-dimethoxyethane; toluene; to soln. of Cr-complex, Cs2CO3 and boronic acid in DME catalyst (mixt. of Pd2(dba)3 and toluene soln. of PMe3) added, mixt. stirred under refluxfor 16 h; ether added, soln. washed (aq. NaOH, H2O, brine), dried (MgSO4), concd. (vac.), flash column chromy (eluant: 15% ether-C6H14); detnd. by elem. anal.;
DOI:10.1039/b006576p