1-((4-methylphenyl)ethynyl)cyclobutanol

Base Information

Chemical Name:1-((4-methylphenyl)ethynyl)cyclobutanol
CAS No.:524742-03-8
Molecular Formula:C₁₃H₁₄O
Molecular Weight:186.254
Hs Code.:

Synonyms:1-((4-methylphenyl)ethynyl)cyclobutanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-((4-methylphenyl)ethynyl)cyclobutanol

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Technology Process of 1-((4-methylphenyl)ethynyl)cyclobutanol

There total 1 articles about 1-((4-methylphenyl)ethynyl)cyclobutanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1191-95-3
cyclobutanone

: 766-97-2
4-n-methylphenylacetylene

: 524742-03-8
1-((4-methylphenyl)ethynyl)cyclobutanol

Guidance literature:: 4-n-methylphenylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

cyclobutanone; In tetrahydrofuran; hexane; at -78 ℃; for 1h;
DOI:10.1021/jo301381z

Reference yield: 96.0%

: 5661-50-7
N-(phenoxy)acetamide

: 524742-03-8
1-((4-methylphenyl)ethynyl)cyclobutanol

: 1-(3-(p-tolyl)benzofuran-2-yl)butan-1-one

Guidance literature:: With dipotassium hydrogenphosphate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; In dichloromethane; at 20 ℃; for 24h; Sealed tube;
DOI:10.1021/acs.orglett.9b00812

Reference yield: 87.0%

: 92-43-3
1-phenylpyrazolidin-3-one

: 524742-03-8
1-((4-methylphenyl)ethynyl)cyclobutanol

: 9-(2-oxopentyl)-9-(p-tolyl)-2,3-dihydro-1H,9H-pyrazolo[1,2-a]indazol-1-one

Guidance literature:: With copper(l) iodide; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium carbonate; In 1,2-dichloro-ethane; at 50 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tetlet.2020.152350