C₂₂H₃₂ClN₃O₇

Base Information

Chemical Name:C₂₂H₃₂ClN₃O₇
CAS No.:1269759-83-2
Molecular Formula:C₂₂H₃₂ClN₃O₇
Molecular Weight:485.965
Hs Code.:

C<sub>22</sub>H<sub>32</sub>ClN<sub>3</sub>O<sub>7</sub>

Synonyms:C₂₂H₃₂ClN₃O₇

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Chemical Property of C₂₂H₃₂ClN₃O₇

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Technology Process of C₂₂H₃₂ClN₃O₇

There total 8 articles about C₂₂H₃₂ClN₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1269759-82-1
C₂₀H₃₁N₃O₆

: 79-04-9
chloroacetyl chloride

: 1269759-83-2
C₂₂H₃₂ClN₃O₇

Guidance literature:: C₂₀H₃₁N₃O₆; With triethylamine; In dichloromethane; Cooling with ice;

chloroacetyl chloride; In dichloromethane; for 0.5h;
DOI:10.1039/c0cc03988h

Reference yield:

: 65710-57-8,81306-93-6
3-{[(benzyloxy)carbonyl]amino}-N-(tert-butoxycarbonyl)-L-alanine

: 1269759-83-2
C₂₂H₃₂ClN₃O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 8.25 h / 20 °C / Cooling with ice

2.1: sodium tetrahydroborate; lithium bromide / tetrahydrofuran; ethanol / 20 °C / Inert atmosphere; Cooling with ice

3.1: triethylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

3.2: 0.67 h / Cooling with ice; Inert atmosphere

4.1: sodium azide / N,N-dimethyl-formamide / 8 h / 55 °C

5.1: hydrogen / methanol / 3.5 h / 20 °C / 1551.49 - 1810.07 Torr

6.1: triethylamine / acetonitrile / 5 h / 20 °C

7.1: triethylamine / dichloromethane / Cooling with ice

7.2: 0.5 h

With sodium tetrahydroborate; sodium azide; hydrogen; potassium carbonate; triethylamine; lithium bromide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c0cc03988h

Reference yield:

: 721927-81-7,1263045-28-8
benzyl tert-butyl [(2S)-3-hydroxypropan-1,2-diyl]biscarbamate

: 1269759-83-2
C₂₂H₃₂ClN₃O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 0.67 h / Cooling with ice; Inert atmosphere

2.1: sodium azide / N,N-dimethyl-formamide / 8 h / 55 °C

3.1: hydrogen / methanol / 3.5 h / 20 °C / 1551.49 - 1810.07 Torr

4.1: triethylamine / acetonitrile / 5 h / 20 °C

5.1: triethylamine / dichloromethane / Cooling with ice

5.2: 0.5 h

With sodium azide; hydrogen; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c0cc03988h