[1-(2-Diphenylamino-phenyl)-1-phenyl-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Base Information

Chemical Name:[1-(2-Diphenylamino-phenyl)-1-phenyl-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester
CAS No.:209412-78-2
Molecular Formula:C₃₁H₃₀N₂O₄
Molecular Weight:494.59
Hs Code.:

Synonyms:[1-(2-Diphenylamino-phenyl)-1-phenyl-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

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Chemical Property of [1-(2-Diphenylamino-phenyl)-1-phenyl-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

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Technology Process of [1-(2-Diphenylamino-phenyl)-1-phenyl-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

There total 3 articles about [1-(2-Diphenylamino-phenyl)-1-phenyl-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16911-31-2
[(2-diphenylamino)phenyl]phenylmethanone

: 209412-78-2
[1-(2-Diphenylamino-phenyl)-1-phenyl-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / NH₂OH*HCl, pyridine / ethanol / 24 h / Heating

2: 64 percent / NaOH / H₂O / 21 h / Heating

3: 1.) CDI / 1.) THF, r.t., 1 h, 2.) THF, light petroleum, 0-5 deg C, 4 h

With pyridine; sodium hydroxide; hydroxylamine hydrochloride; 1,1'-carbonyldiimidazole; In ethanol; water;
DOI:10.1039/a800868j

Reference yield:

: (2-Diphenylamino-phenyl)-phenyl-methanone oxime

: 209412-78-2
[1-(2-Diphenylamino-phenyl)-1-phenyl-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / NaOH / H₂O / 21 h / Heating

2: 1.) CDI / 1.) THF, r.t., 1 h, 2.) THF, light petroleum, 0-5 deg C, 4 h

With sodium hydroxide; 1,1'-carbonyldiimidazole; In water;
DOI:10.1039/a800868j

Reference yield:

: 75-91-2
tert.-butylhydroperoxide

: [1-(2-Diphenylamino-phenyl)-1-phenyl-meth-(E)-ylideneaminooxy]-acetic acid

: 209412-78-2
[1-(2-Diphenylamino-phenyl)-1-phenyl-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Guidance literature:: With 1,1'-carbonyldiimidazole; Yield given. Multistep reaction; 1.) THF, r.t., 1 h, 2.) THF, light petroleum, 0-5 deg C, 4 h;
DOI:10.1039/a800868j