N₁-[(5''-acetoxyethoxy)methyl]-N₉-[(5'-tert-butyldiphenylsilyloxyethoxy)methyl]-8-bromohypoxanthine

Base Information

• Chemical Name: N₁-[(5''-acetoxyethoxy)methyl]-N₉-[(5'-tert-butyldiphenylsilyloxyethoxy)methyl]-8-bromohypoxanthine
• CAS No.: 1256827-34-5
• Molecular Formula: C₂₉H₃₅BrN₄O₆Si
• Molecular Weight: 643.61

Synonyms:N₁-[(5''-acetoxyethoxy)methyl]-N₉-[(5'-tert-butyldiphenylsilyloxyethoxy)methyl]-8-bromohypoxanthine

Chemical Property of N₁-[(5''-acetoxyethoxy)methyl]-N₉-[(5'-tert-butyldiphenylsilyloxyethoxy)methyl]-8-bromohypoxanthine

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Technology Process of N₁-[(5''-acetoxyethoxy)methyl]-N₉-[(5'-tert-butyldiphenylsilyloxyethoxy)methyl]-8-bromohypoxanthine

There total 1 articles about N₁-[(5''-acetoxyethoxy)methyl]-N₉-[(5'-tert-butyldiphenylsilyloxyethoxy)methyl]-8-bromohypoxanthine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

1-acetoxy-2-chloromethoxyethane (40510-88-1) + N9-[(5'-tert-butyldiphenylsilyloxyethoxy)methyl]-8-bromohypoxanthine (1256827-33-4) → N1-[(5''-acetoxyethoxy)methyl]-N9-[(5'-tert-butyldiphenylsilyloxyethoxy)methyl]-8-bromohypoxanthine (1256827-34-5) + C29H35BrN4O6Si

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 20 ℃;

DOI:10.3390/molecules15128689

Reference yield: 42.0%

2,2-difluoro-2-(fluorosulfonyl)acetate (680-15-9) + N1-[(5''-acetoxyethoxy)methyl]-N9-[(5'-tert-butyldiphenylsilyloxyethoxy)methyl]-8-bromohypoxanthine (1256827-34-5) → N1-[(5''-acetoxyethoxy)methyl]-N9-[(5'-hydroxylethoxy)methyl]-8-trifluoromethylhypoxanthine (1256827-36-7) + N1-[(5''-acetoxyethoxy)methyl]-N9-[(5'-tert-butyldiphenylsilyloxyethoxy)methyl]-8-trifluoromethylhypoxanthine (1256827-35-6)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; In N,N-dimethyl-formamide; at 70 ℃; for 20h; Inert atmosphere;

DOI:10.3390/molecules15128689

upstream raw materials:

1-acetoxy-2-chloromethoxyethane

N₉-[(5'-tert-butyldiphenylsilyloxyethoxy)methyl]-8-bromohypoxanthine

Downstream raw materials:

N₁-[(5''-acetoxyethoxy)methyl]-N₉-[(5'-hydroxylethoxy)methyl]-8-trifluoromethylhypoxanthine

N₁-[(5''-acetoxyethoxy)methyl]-N₉-[(5'-tert-butyldiphenylsilyloxyethoxy)methyl]-8-trifluoromethylhypoxanthine

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