Technology Process of C19H26ClN3O2S
There total 6 articles about C19H26ClN3O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C19H27ClN2O4S;
With
ammonium acetate; acetic acid;
for 8h;
Reflux;
With
sodium hydrogencarbonate;
In
water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride / ethanol; water / 3 h / 0 - 50 °C
2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C
2.2: 0 - 20 °C
3.1: ammonium acetate; acetic acid / 8 h / Reflux
With
hydrogenchloride; oxalyl dichloride; ammonium acetate; acetic acid;
N,N-dimethyl-formamide;
In
ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: chloroform / 2 h / 0 - 50 °C
2.1: hydrogenchloride / ethanol; water / 3 h / 0 - 50 °C
3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C
3.2: 0 - 20 °C
4.1: ammonium acetate; acetic acid / 8 h / Reflux
With
hydrogenchloride; oxalyl dichloride; ammonium acetate; acetic acid;
N,N-dimethyl-formamide;
In
ethanol; dichloromethane; chloroform; water;