1--3-hydroxypyridinium chloride

Base Information

Chemical Name:1--3-hydroxypyridinium chloride
CAS No.:74780-45-3
Molecular Formula:C₁₄H₁₀ClN₂O₄*Cl
Molecular Weight:341.15
Hs Code.:

1-<trans-3-(2-chloro-5-nitrophenyl)-3-oxoprop-1-enyl>-3-hydroxypyridinium chloride

Synonyms:1--3-hydroxypyridinium chloride

Suppliers and Price of 1--3-hydroxypyridinium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1--3-hydroxypyridinium chloride

Chemical Property:

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Technology Process of 1--3-hydroxypyridinium chloride

There total 1 articles about 1--3-hydroxypyridinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 109-00-2
3-HYDROXYPYRIDINE

: 74780-46-4
trans-1-(2-chloro-5-nitrophenyl)-3-chloroprop-2-en-1-one

: 74780-45-3
1--3-hydroxypyridinium chloride

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1039/P19800000362

Reference yield: 87.0%

: 74780-45-3
1--3-hydroxypyridinium chloride

: 74780-52-2
3,11-bis--3,11-diazatricyclo<5.3.1.1^2,6>dodeca-4,8-diene-10,12-dione

Guidance literature:: With triethylamine; In acetonitrile; for 0.166667h;
DOI:10.1039/P19800000362

Reference yield:

: 74780-45-3
1--3-hydroxypyridinium chloride

: 74780-56-6,74780-57-7
8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / triethylamine / acetonitrile / 0.17 h

2: hydroquinone / tetrahydrofuran; chlorobenzene / 48 h / 110 - 130 °C

With triethylamine; hydroquinone; In tetrahydrofuran; chlorobenzene; acetonitrile;
DOI:10.1039/P19800000362