trans-{Rh(1,3,4,6-tetrakis(7-(1-imidazolyl)-2,5-dioxaheptyl)tetrahydro-3a,6a-diphenylimidazo(4,5-d)imidazole-2,5(1H,3H)-dione)Cl₂}Cl*6.4H₂O

Base Information

• Chemical Name: trans-{Rh(1,3,4,6-tetrakis(7-(1-imidazolyl)-2,5-dioxaheptyl)tetrahydro-3a,6a-diphenylimidazo(4,5-d)imidazole-2,5(1H,3H)-dione)Cl₂}Cl*6.4H₂O
• CAS No.: 101333-07-7
• Molecular Formula: C₄₈H₆₂Cl₂N₁₂O₁₀Rh*Cl*6H₂O
• Molecular Weight: 1291.66

Synonyms:trans-{Rh(1,3,4,6-tetrakis(7-(1-imidazolyl)-2,5-dioxaheptyl)tetrahydro-3a,6a-diphenylimidazo(4,5-d)imidazole-2,5(1H,3H)-dione)Cl₂}Cl*6.4H₂O

Chemical Property of trans-{Rh(1,3,4,6-tetrakis(7-(1-imidazolyl)-2,5-dioxaheptyl)tetrahydro-3a,6a-diphenylimidazo(4,5-d)imidazole-2,5(1H,3H)-dione)Cl₂}Cl*6.4H₂O

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Technology Process of trans-{Rh(1,3,4,6-tetrakis(7-(1-imidazolyl)-2,5-dioxaheptyl)tetrahydro-3a,6a-diphenylimidazo(4,5-d)imidazole-2,5(1H,3H)-dione)Cl₂}Cl*6.4H₂O

There total 1 articles about trans-{Rh(1,3,4,6-tetrakis(7-(1-imidazolyl)-2,5-dioxaheptyl)tetrahydro-3a,6a-diphenylimidazo(4,5-d)imidazole-2,5(1H,3H)-dione)Cl₂}Cl*6.4H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

rhodium(III) chloride trihydrate + 1,3,4,6-tetrakis(7-(1-imidazolyl)-2,5-dioxaheptyl)tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione (101241-23-0) → trans-{Rh(1,3,4,6-tetrakis(7-(1-imidazolyl)-2,5-dioxaheptyl)tetrahydro-3a,6a-diphenylimidazo(4,5-d)imidazole-2,5(1H,3H)-dione)Cl2}Cl*6.4H2O (101333-07-7)

Guidance literature:

In methanol; stirring (48 h); filtration and evapn. in vac., elem. anal.;

DOI:10.1021/ja00188a022

upstream raw materials:

1,3,4,6-tetrakis(7-(1-imidazolyl)-2,5-dioxaheptyl)tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione

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