Imidazo[4,5-d]imidazole-2,5(1H,3H)-dione, tetrahydro-1,3,4,6-tetrakis[[2-[2-(1H-imidazol-1-yl)ethoxy]ethoxy]methyl]- 3a,6a-diphenyl-, cis-

Base Information

Chemical Name:Imidazo[4,5-d]imidazole-2,5(1H,3H)-dione, tetrahydro-1,3,4,6-tetrakis[[2-[2-(1H-imidazol-1-yl)ethoxy]ethoxy]methyl]- 3a,6a-diphenyl-, cis-
CAS No.:101241-23-0
Molecular Formula:C48H62N12O10
Molecular Weight:967.095
Hs Code.:
Mol file:101241-23-0.mol

Synonyms:

Suppliers and Price of Imidazo[4,5-d]imidazole-2,5(1H,3H)-dione, tetrahydro-1,3,4,6-tetrakis[[2-[2-(1H-imidazol-1-yl)ethoxy]ethoxy]methyl]- 3a,6a-diphenyl-, cis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Imidazo[4,5-d]imidazole-2,5(1H,3H)-dione, tetrahydro-1,3,4,6-tetrakis[[2-[2-(1H-imidazol-1-yl)ethoxy]ethoxy]methyl]- 3a,6a-diphenyl-, cis-

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Imidazo[4,5-d]imidazole-2,5(1H,3H)-dione, tetrahydro-1,3,4,6-tetrakis[[2-[2-(1H-imidazol-1-yl)ethoxy]ethoxy]methyl]- 3a,6a-diphenyl-, cis-

There total 4 articles about Imidazo[4,5-d]imidazole-2,5(1H,3H)-dione, tetrahydro-1,3,4,6-tetrakis[[2-[2-(1H-imidazol-1-yl)ethoxy]ethoxy]methyl]- 3a,6a-diphenyl-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101241-21-8
3a,6a-diphenylglycoluril

: 101241-23-0
1,3,4,6-tetrakis<7-(1-imidazolyl)-2,5-dioxaheptyl>tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / 1M aqueous NaOH / dimethylsulfoxide / 16 h / Ambient temperature; pH = 9

2: 56 percent / p-toluenesulfonic acid monohydrate / toluene / 60 h / Heating

3: dimethylformamide / 16 h / 80 °C

With sodium hydroxide; toluene-4-sulfonic acid; In dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja00209a027

Reference yield:

: 101241-22-9
1,3,4,6-tetrakis(hydroxymethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

: 101241-23-0
1,3,4,6-tetrakis<7-(1-imidazolyl)-2,5-dioxaheptyl>tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / p-toluenesulfonic acid monohydrate / toluene / 60 h / Heating

2: dimethylformamide / 16 h / 80 °C

With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja00209a027