7-chloro-3-(2-hydroxy-ethyl)-5-phenyl-1,3-dihydro-benzo[e][1,2,4]triazepine-2-thione

Base Information

Chemical Name:7-chloro-3-(2-hydroxy-ethyl)-5-phenyl-1,3-dihydro-benzo[e][1,2,4]triazepine-2-thione
CAS No.:67862-90-2
Molecular Formula:C₁₆H₁₄ClN₃OS
Molecular Weight:331.826
Hs Code.:

7-chloro-3-(2-hydroxy-ethyl)-5-phenyl-1,3-dihydro-benzo[<i>e</i>][1,2,4]triazepine-2-thione

Synonyms:7-chloro-3-(2-hydroxy-ethyl)-5-phenyl-1,3-dihydro-benzo[e][1,2,4]triazepine-2-thione

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Chemical Property of 7-chloro-3-(2-hydroxy-ethyl)-5-phenyl-1,3-dihydro-benzo[e][1,2,4]triazepine-2-thione

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Technology Process of 7-chloro-3-(2-hydroxy-ethyl)-5-phenyl-1,3-dihydro-benzo[e][1,2,4]triazepine-2-thione

There total 1 articles about 7-chloro-3-(2-hydroxy-ethyl)-5-phenyl-1,3-dihydro-benzo[e][1,2,4]triazepine-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67862-90-2
7-chloro-3-(2-hydroxy-ethyl)-5-phenyl-1,3-dihydro-benzo[e][1,2,4]triazepine-2-thione

Guidance literature:: aus N-(2-Benzoyl-4-chlorphenyl)-β-hydroxy-aethyl-hydrazin-carbothioamid, Δ;

Reference yield: 65.0%

: 67862-90-2
7-chloro-3-(2-hydroxy-ethyl)-5-phenyl-1,3-dihydro-benzo[e][1,2,4]triazepine-2-thione

: 86230-82-2
7-chloro-9-phenyl-1,2-dihydrooxazolo<2,3-b>-1,3,4-benzotriazepine

Guidance literature:: With dihydrogen peroxide; sodium methylate; In methanol; water; acetone; for 2h; Ambient temperature;

Reference yield:

: 67862-90-2
7-chloro-3-(2-hydroxy-ethyl)-5-phenyl-1,3-dihydro-benzo[e][1,2,4]triazepine-2-thione

: 86230-83-3
7-Chlor-3-(2-iodethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaOCH₃ (1 mol/l), 30percent H₂O₂ / acetone; H₂O; methanol / 2 h / Ambient temperature

2: 80 percent / 43percent HI / dioxane; H₂O / 48 h / Ambient temperature

With hydrogen iodide; dihydrogen peroxide; sodium methylate; In 1,4-dioxane; methanol; water; acetone;