(3aα,4β,6aα)-1,3-dibenzylhexahydro-4-(3-methoxypropyl)-1H-thieno<3,4-d>imidazol-2(3H)-one

Base Information

Chemical Name:(3aα,4β,6aα)-1,3-dibenzylhexahydro-4-(3-methoxypropyl)-1H-thieno<3,4-d>imidazol-2(3H)-one
CAS No.:288392-52-9
Molecular Formula:C₂₃H₂₈N₂O₂S
Molecular Weight:396.554
Hs Code.:

Synonyms:(3aα,4β,6aα)-1,3-dibenzylhexahydro-4-(3-methoxypropyl)-1H-thieno<3,4-d>imidazol-2(3H)-one

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Chemical Property of (3aα,4β,6aα)-1,3-dibenzylhexahydro-4-(3-methoxypropyl)-1H-thieno<3,4-d>imidazol-2(3H)-one

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Technology Process of (3aα,4β,6aα)-1,3-dibenzylhexahydro-4-(3-methoxypropyl)-1H-thieno<3,4-d>imidazol-2(3H)-one

There total 3 articles about (3aα,4β,6aα)-1,3-dibenzylhexahydro-4-(3-methoxypropyl)-1H-thieno<3,4-d>imidazol-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.6%

: C₂₃H₂₆N₂O₂S

: 288392-52-9
(3aα,4β,6aα)-1,3-dibenzylhexahydro-4-(3-methoxypropyl)-1H-thieno<3,4-d>imidazol-2(3H)-one

Guidance literature:: C₂₃H₂₆N₂O₂S; In methanol; at 20 ℃;

With hydrogen; sodium acetate; palladium(II) hydroxide; In methanol; at 20 ℃; under 3000.3 - 3750.38 Torr; Reagent/catalyst; Temperature; Autoclave;

Reference yield:

: 28092-54-8
(3aS)-1,3-dibenzyl-6-(3-methoxy-propylidene)-(3ar,6ac)-tetrahydro-thieno[3,4-d]imidazol-2-one

: 288392-52-9
(3aα,4β,6aα)-1,3-dibenzylhexahydro-4-(3-methoxypropyl)-1H-thieno<3,4-d>imidazol-2(3H)-one

Guidance literature:: With hydrogen; nickel; under 30400 Torr;
DOI:10.1002/hlca.19700530514

Reference yield:

: 28092-53-7
(3aS)-1,3-dibenzyl-4ξ-hydroxy-4ξ-(3-methoxy-propyl)-(3ar,6ac)-tetrahydro-thieno[3,4-d]imidazol-2-one

: 288392-52-9
(3aα,4β,6aα)-1,3-dibenzylhexahydro-4-(3-methoxypropyl)-1H-thieno<3,4-d>imidazol-2(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH / Heating

2: H₂ / Raney-Ni / 30400 Torr

With hydrogen; acetic acid; nickel;
DOI:10.1002/hlca.19700530514