Technology Process of C29H26F3NOS
There total 5 articles about C29H26F3NOS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tri tert-butylphosphoniumtetrafluoroborate;
In
water; toluene;
at 90 ℃;
for 14h;
optical yield given as %de;
diastereoselective reaction;
DOI:10.1016/j.tetlet.2012.02.096
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: magnesium sulfate / tetrahydrofuran / 0 °C
2.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C
2.2: 0 - 20 °C
3.1: tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate; tri tert-butylphosphoniumtetrafluoroborate / water; toluene / 14 h / 90 °C
With
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); sodium hexamethyldisilazane; magnesium sulfate; tri tert-butylphosphoniumtetrafluoroborate;
In
tetrahydrofuran; water; toluene;
3.1: Heck-Suzuki cascade reaction;
DOI:10.1016/j.tetlet.2012.02.096
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C
1.2: 0 - 20 °C
2.1: tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate; tri tert-butylphosphoniumtetrafluoroborate / water; toluene / 14 h / 90 °C
With
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); sodium hexamethyldisilazane; tri tert-butylphosphoniumtetrafluoroborate;
In
tetrahydrofuran; water; toluene;
2.1: Heck-Suzuki cascade reaction;
DOI:10.1016/j.tetlet.2012.02.096
