3-{3,4,5-tris[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionic acid

Base Information

Chemical Name:3-{3,4,5-tris[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionic acid
CAS No.:883196-35-8
Molecular Formula:C₇₂H₁₁₂O₈
Molecular Weight:1105.68
Hs Code.:

Synonyms:3-{3,4,5-tris[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionic acid

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Chemical Property of 3-{3,4,5-tris[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionic acid

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Technology Process of 3-{3,4,5-tris[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionic acid

There total 15 articles about 3-{3,4,5-tris[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 883196-32-5
methyl 3-{3,4,5-tris[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionate

: 883196-35-8
3-{3,4,5-tris[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionic acid

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; ethanol; water; Heating;
DOI:10.1021/ja060062a

Reference yield:

: 5597-50-2
3-(4-hydroxyphenyl)propionic acid methyl ester

: 883196-35-8
3-{3,4,5-tris[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / K₂CO₃ / dimethylformamide / 12 h / 80 °C

2: 96 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / 0 °C

3: 91 percent / CBr₄; PPh₃ / CH₂Cl₂ / 2 h / 0 °C

4: 89 percent / K₂CO₃ / dimethylformamide / 20 h / 80 °C

5: 88 percent / KOH / ethanol; tetrahydrofuran; H₂O / Heating

With potassium hydroxide; lithium aluminium tetrahydride; carbon tetrabromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja060062a

Reference yield:

: propyl 3,4,5-tris(benzyloxy)benzoate

: 883196-35-8
3-{3,4,5-tris[3-(4-dodecyl-1-oxyphenyl)propyl-1-oxy]phenyl}propionic acid

Guidance literature:: Multi-step reaction with 7 steps

1: 95 percent / LiAlH₄ / tetrahydrofuran / 0 - 20 °C

2: pyridinium chlorochromate / CH₂Cl₂ / 20 °C

3: 94 percent / morpholine; AcOH / Heating

4: 94 percent / p-toluenesulfonic acid monohydrate / 24 h / Heating

5: 92 percent / H₂ / Pd/C / ethanol

6: 89 percent / K₂CO₃ / dimethylformamide / 20 h / 80 °C

7: 88 percent / KOH / ethanol; tetrahydrofuran; H₂O / Heating

With morpholine; potassium hydroxide; lithium aluminium tetrahydride; hydrogen; potassium carbonate; toluene-4-sulfonic acid; acetic acid; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; 3: Knoevenagel condensation;
DOI:10.1021/ja060062a