8-(3-butoxycarbonylphenyl)-(3',5'-bis-O-(6-bromopentanoyl))-2'-deoxyguanosine

Base Information

Chemical Name:8-(3-butoxycarbonylphenyl)-(3',5'-bis-O-(6-bromopentanoyl))-2'-deoxyguanosine
CAS No.:1426244-65-6
Molecular Formula:C₃₁H₃₉Br₂N₅O₈
Molecular Weight:769.487
Hs Code.:

Synonyms:8-(3-butoxycarbonylphenyl)-(3',5'-bis-O-(6-bromopentanoyl))-2'-deoxyguanosine

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Chemical Property of 8-(3-butoxycarbonylphenyl)-(3',5'-bis-O-(6-bromopentanoyl))-2'-deoxyguanosine

Chemical Property:

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Technology Process of 8-(3-butoxycarbonylphenyl)-(3',5'-bis-O-(6-bromopentanoyl))-2'-deoxyguanosine

There total 4 articles about 8-(3-butoxycarbonylphenyl)-(3',5'-bis-O-(6-bromopentanoyl))-2'-deoxyguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2067-33-6
5-bromopentanoic acid

: 1426244-64-5
8-(3-butoxycarbonylphenyl)-2'-deoxyguanosine

: 1426244-65-6
8-(3-butoxycarbonylphenyl)-(3',5'-bis-O-(6-bromopentanoyl))-2'-deoxyguanosine

Guidance literature:: With dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In N,N-dimethyl-formamide;
DOI:10.1021/ja401373h

Reference yield:

: 25487-66-5
3-Carboxyphenylboronic acid

: 1426244-65-6
8-(3-butoxycarbonylphenyl)-(3',5'-bis-O-(6-bromopentanoyl))-2'-deoxyguanosine

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate / N,N-dimethyl-formamide

2: trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; sodium carbonate / water; acetonitrile / 80 °C

3: dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate / N,N-dimethyl-formamide

With trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; sodium carbonate; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In water; N,N-dimethyl-formamide; acetonitrile; 2: |Suzuki Coupling;
DOI:10.1021/ja401373h

Reference yield:

: 13389-03-2
8-bromo-2'-deoxyguanosine

: 1426244-65-6
8-(3-butoxycarbonylphenyl)-(3',5'-bis-O-(6-bromopentanoyl))-2'-deoxyguanosine

Guidance literature:: Multi-step reaction with 2 steps

1: trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; sodium carbonate / water; acetonitrile / 80 °C

2: dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate / N,N-dimethyl-formamide

With trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; sodium carbonate; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In water; N,N-dimethyl-formamide; acetonitrile; 1: |Suzuki Coupling;
DOI:10.1021/ja401373h