2,4-Dichloro-6-pyren-1-yl-1,3,5-triazine

Base Information

• Chemical Name: 2,4-Dichloro-6-pyren-1-yl-1,3,5-triazine
• CAS No.: 3224-36-0
• Molecular Formula: C19H9 Cl2 N3
• Molecular Weight: 350.207
• Hs Code.: 2933699090
• European Community (EC) Number: 221-754-9
• DSSTox Substance ID: DTXSID90185996
• Nikkaji Number: J262.332C
• Wikidata: Q83057179
• Mol file: 3224-36-0.mol

Synonyms:3224-36-0;PyTC2;2,4-Dichloro-6-pyren-1-yl-1,3,5-triazine;1-(Dichloro-1,3,5-triazinyl)-pyrene;1-(4,6-Dichloro-1,3,5-triazin-2-yl)pyrene;EINECS 221-754-9;2,4-dichloro-6-(pyren-1-yl)-1,3,5-triazine;1,3,5-Triazine,2,4-dichloro-6-(1-pyrenyl)-;PyTC2 [1-(4,6-Dichloro-1,3,5-triazin-2-yl)pyrene];C19H9Cl2N3;SCHEMBL2054216;C19-H9-Cl2-N3;DTXSID90185996;MFCD08276990;2,4-Dichloro-6-(1-pyrenyl)-1,3,5-triazine;1-(4,6-Dichloro-1,3,5-triazin-2-yl)pyrene, BioReagent, suitable for fluorescence, >=85% (HPCE)

Chemical Property of 2,4-Dichloro-6-pyren-1-yl-1,3,5-triazine

Chemical Property:

• Vapor Pressure: 5.05E-15mmHg at 25°C
• Boiling Point: 628.4°Cat760mmHg
• Flash Point: 359.3°C
• PSA: 38.67000
• Density: 1.517g/cm³
• LogP: 5.74280
• Solubility.: chloroform: soluble
• XLogP3: 6.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 349.0173527
• Heavy Atom Count: 24
• Complexity: 466

Purity/Quality:

1-(4,6-Dichloro-1,3,5-triazin-2-yl)pyrene ^*data from reagent suppliers

Safty Information:

• Hazard Codes: T,N
• Statements: 25-36/37/38-50/53
• Safety Statements: 26-45-60-61

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC2=C3C(=C1)C=CC4=C(C=CC(=C43)C=C2)C5=NC(=NC(=N5)Cl)Cl
• Uses: 1-(4,6-Dichloro-1,3,5-triazin-2-yl)pyrene (cas# 3224-36-0) is a compound useful in organic synthesis.

Technology Process of 2,4-Dichloro-6-pyren-1-yl-1,3,5-triazine

There total 2 articles about 2,4-Dichloro-6-pyren-1-yl-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1,3,5-trichloro-2,4,6-triazine (108-77-0) + pyrene (129-00-0) → 2,4-dichloro-6-(pyren-1-yl)-1,3,5-triazine (3224-36-0)

Guidance literature:

With aluminum (III) chloride; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/jacs.5b04643

Reference yield:

pyrene (129-00-0) → 2,4-dichloro-6-(pyren-1-yl)-1,3,5-triazine (3224-36-0)

Guidance literature:

1,3,5-trichloro-2,4,6-triazine; With aluminum (III) chloride; In 1,2-dichloro-benzene; at 0 - 5 ℃; for 0.5h;

pyrene; In 1,2-dichloro-benzene; at 0 ℃; for 3h; Product distribution / selectivity;

upstream raw materials:

1,3,5-trichloro-2,4,6-triazine

pyrene