C₂₂H₃₄O₄Si

Base Information

Chemical Name:C₂₂H₃₄O₄Si
CAS No.:1264756-56-0
Molecular Formula:C₂₂H₃₄O₄Si
Molecular Weight:390.595
Hs Code.:

C<sub>22</sub>H<sub>34</sub>O<sub>4</sub>Si

Synonyms:C₂₂H₃₄O₄Si

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Chemical Property of C₂₂H₃₄O₄Si

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Technology Process of C₂₂H₃₄O₄Si

There total 1 articles about C₂₂H₃₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 994-30-9
triethylsilyl chloride

: 131310-61-7
(2R,4aR,6S,7R,8aS)-6-Methyl-2-phenyl-6-vinyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol

: 1264756-56-0
C₂₂H₃₄O₄Si

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield: 96.0%

: 1264756-56-0
C₂₂H₃₄O₄Si

: 1264756-54-8
C₂₁H₃₂O₅Si

Guidance literature:: C₂₂H₃₄O₄Si; With ozone; In dichloromethane; at -78 ℃;

With triphenylphosphine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield:

: 1264756-56-0
C₂₂H₃₄O₄Si

: 1264756-73-1
C₄₁H₆₀O₉Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: ozone / dichloromethane / -78 °C

1.2: -78 - 20 °C

2.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / diethyl ether / 0 °C

2.2: -78 °C

3.1: Dess-Martin periodane / dichloromethane; tert-butyl alcohol / 20 °C

4.1: pyridinium p-toluenesulfonate / methanol / 80 °C

5.1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 20 °C

6.1: sodium tetrahydroborate; cerium(III) chloride / methanol; dichloromethane / 0 °C

7.1: boron trifluoride tetrahydrofuran complex / tetrahydrofuran / 0 °C

7.2: 0 - 20 °C

8.1: 2,6-dimethylpyridine / dichloromethane / 20 °C

9.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0 °C

10.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

11.1: toluene-4-sulfonic acid / methanol; dichloromethane / 20 °C

12.1: triethylsilane; trimethylsilyl trifluoromethanesulfonate / propiononitrile / -78 °C

With 2,6-dimethylpyridine; triethylsilane; sodium tetrahydroborate; cerium(III) chloride; tetrapropylammonium perruthennate; boron trifluoride tetrahydrofuran complex; trimethylsilyl trifluoromethanesulfonate; di-n-butylboryl trifluoromethanesulfonate; water; pyridinium p-toluenesulfonate; Dess-Martin periodane; toluene-4-sulfonic acid; ozone; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; propiononitrile; tert-butyl alcohol; 3.1: Dess-Martin oxidation / 6.1: Luche reduction;
DOI:10.1016/j.tetlet.2010.11.127