2-(4-phenyl-2-tosyl-1,2-dihydrophthalazin-1-yl)-1-(piperidin-1-yl)ethanone

Base Information

Chemical Name:2-(4-phenyl-2-tosyl-1,2-dihydrophthalazin-1-yl)-1-(piperidin-1-yl)ethanone
CAS No.:1402416-38-9
Molecular Formula:C₂₈H₂₉N₃O₃S
Molecular Weight:487.623
Hs Code.:

Synonyms:2-(4-phenyl-2-tosyl-1,2-dihydrophthalazin-1-yl)-1-(piperidin-1-yl)ethanone

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Chemical Property of 2-(4-phenyl-2-tosyl-1,2-dihydrophthalazin-1-yl)-1-(piperidin-1-yl)ethanone

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Technology Process of 2-(4-phenyl-2-tosyl-1,2-dihydrophthalazin-1-yl)-1-(piperidin-1-yl)ethanone

There total 3 articles about 2-(4-phenyl-2-tosyl-1,2-dihydrophthalazin-1-yl)-1-(piperidin-1-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 10043-37-5
N-acrylpiperidine

: 4545-20-4
benzophenone tosylhydrazone

: 1402416-38-9
2-(4-phenyl-2-tosyl-1,2-dihydrophthalazin-1-yl)-1-(piperidin-1-yl)ethanone

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In N,N-dimethyl-formamide; at 80 ℃; for 24h; Sealed tube; Inert atmosphere;
DOI:10.1021/ol302522n

Reference yield:

: 119-61-9
benzophenone

: 1402416-38-9
2-(4-phenyl-2-tosyl-1,2-dihydrophthalazin-1-yl)-1-(piperidin-1-yl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water; methanol / 1 h / Reflux

2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate / N,N-dimethyl-formamide / 24 h / 80 °C / Sealed tube; Inert atmosphere

With hydrogenchloride; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ol302522n

Reference yield:

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1402416-38-9
2-(4-phenyl-2-tosyl-1,2-dihydrophthalazin-1-yl)-1-(piperidin-1-yl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water; methanol / 1 h / Reflux

2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate / N,N-dimethyl-formamide / 24 h / 80 °C / Sealed tube; Inert atmosphere

With hydrogenchloride; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ol302522n