4,4'-(Thiodi-2,1-cyclohexanediyl)bismorpholine

Base Information

Chemical Name:4,4'-(Thiodi-2,1-cyclohexanediyl)bismorpholine
CAS No.:73477-72-2
Molecular Formula:C20H36N2O2S
Molecular Weight:368.584
Hs Code.:
DSSTox Substance ID:DTXSID00994233

Synonyms:2,2'-Dimorpholinyldicyclohexylsulfide;4,4'-(Thiodi-2,1-cyclohexanediyl)bismorpholine;Morpholine, 4,4'-(thiodi-2,1-cyclohexanediyl)bis-;73477-72-2;C20H36N2O2S;DTXSID00994233;C20-H36-N2-O2-S;LS-93454;4,4'-[Sulfanediyldi(cyclohexane-2,1-diyl)]bis(morpholine)

Suppliers and Price of 4,4'-(Thiodi-2,1-cyclohexanediyl)bismorpholine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 4,4'-(Thiodi-2,1-cyclohexanediyl)bismorpholine

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:368.24974957
Heavy Atom Count:25
Complexity:363

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(C(C1)N2CCOCC2)SC3CCCCC3N4CCOCC4

Technology Process of 4,4'-(Thiodi-2,1-cyclohexanediyl)bismorpholine

There total 2 articles about 4,4'-(Thiodi-2,1-cyclohexanediyl)bismorpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 110-91-8,99108-56-2
morpholine

: 52612-19-8
2,2'-dichlorodicyclohexylsulfide

: 73477-72-2
2,2-dimorpholinyldicyclohexylsulfide

Guidance literature:: at 120 - 150 ℃; for 6h;
DOI:10.1007/BF02219203

Reference yield:

: 110-83-8
cyclohexene

: 73477-72-2
2,2-dimorpholinyldicyclohexylsulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / SCl₂ / CH₂Cl₂ / 2 h / Ambient temperature

2: 86 percent / 6 h / 120 - 150 °C

With sulfur dichloride; In dichloromethane;
DOI:10.1007/BF02219203