(5S)-5-methyl-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamino]-2,5-dihydro-1H-2-azolone

Base Information

Chemical Name:(5S)-5-methyl-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamino]-2,5-dihydro-1H-2-azolone
CAS No.:474888-45-4
Molecular Formula:C₂₁H₂₄N₂O
Molecular Weight:320.434
Hs Code.:

Synonyms:(5S)-5-methyl-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamino]-2,5-dihydro-1H-2-azolone

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Chemical Property of (5S)-5-methyl-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamino]-2,5-dihydro-1H-2-azolone

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Technology Process of (5S)-5-methyl-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamino]-2,5-dihydro-1H-2-azolone

There total 3 articles about (5S)-5-methyl-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamino]-2,5-dihydro-1H-2-azolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 474888-42-1
5-methylene-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamine]-2,5-dihydro-1H-2-azolone

: (R)-5-Methyl-1-((S)-1-phenyl-ethyl)-4-((S)-1-phenyl-ethylamino)-1,5-dihydro-pyrrol-2-one

: 474888-45-4
(5S)-5-methyl-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamino]-2,5-dihydro-1H-2-azolone

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 25 ℃;
DOI:10.1021/ol026599k

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 474888-45-4
(5S)-5-methyl-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamino]-2,5-dihydro-1H-2-azolone

Guidance literature:: Multi-step reaction with 3 steps

1: 98percent HCO₂H; 4 Angstroem molecular sieves / CH₂Cl₂ / 168 h / 25 °C

2: 51 percent / boron trifluoride / tetrahydrofuran / Heating

3: 60 percent / H₂ / 10 percent Pd/C / methanol / 25 °C / atmospheric pressure

With 4 A molecular sieve; boron trifluoride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol026599k

Reference yield:

: 67122-56-9
(S,S)-N,N'-(1,2-dimethylethanediylidene)bis(α-methylbenzenemethylamine)

: 474888-45-4
(5S)-5-methyl-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamino]-2,5-dihydro-1H-2-azolone

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / boron trifluoride / tetrahydrofuran / Heating

2: 60 percent / H₂ / 10 percent Pd/C / methanol / 25 °C / atmospheric pressure

With boron trifluoride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/ol026599k