5-methylene-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamine]-2,5-dihydro-1H-2-azolone

Base Information

Chemical Name:5-methylene-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamine]-2,5-dihydro-1H-2-azolone
CAS No.:474888-42-1
Molecular Formula:C₂₁H₂₂N₂O
Molecular Weight:318.418
Hs Code.:

Synonyms:5-methylene-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamine]-2,5-dihydro-1H-2-azolone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-methylene-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamine]-2,5-dihydro-1H-2-azolone

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Technology Process of 5-methylene-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamine]-2,5-dihydro-1H-2-azolone

There total 1 articles about 5-methylene-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamine]-2,5-dihydro-1H-2-azolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 530-62-1
1,1'-carbonyldiimidazole

: 67122-56-9
(S,S)-N,N'-(1,2-dimethylethanediylidene)bis(α-methylbenzenemethylamine)

: 474888-42-1
5-methylene-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamine]-2,5-dihydro-1H-2-azolone

Guidance literature:: With boron trifluoride; In tetrahydrofuran; Heating;
DOI:10.1021/ol026599k

Reference yield: 60.0%

: 474888-42-1
5-methylene-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamine]-2,5-dihydro-1H-2-azolone

: (R)-5-Methyl-1-((S)-1-phenyl-ethyl)-4-((S)-1-phenyl-ethylamino)-1,5-dihydro-pyrrol-2-one

: 474888-45-4
(5S)-5-methyl-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamino]-2,5-dihydro-1H-2-azolone

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 25 ℃;
DOI:10.1021/ol026599k

Reference yield:

: 474888-42-1
5-methylene-1-[(1S)-1-phenylethyl]-4-[(1S)-1-phenylethylamine]-2,5-dihydro-1H-2-azolone

: 474888-35-2
(5S)-5-methyl-1-[(1S)-1-phenylethyl]-azolane-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / H₂ / 10 percent Pd/C / methanol / 25 °C / atmospheric pressure

2: 90 percent / 6N aq. H₂SO₄ / diethyl ether / 7 h / 20 °C

With sulfuric acid; hydrogen; palladium on activated charcoal; In methanol; diethyl ether;
DOI:10.1021/ol026599k