C₄₈H₃₀N₂O

Base Information

Chemical Name:C₄₈H₃₀N₂O
CAS No.:1428635-33-9
Molecular Formula:C₄₈H₃₀N₂O
Molecular Weight:650.779
Hs Code.:

C<sub>48</sub>H<sub>30</sub>N<sub>2</sub>O

Synonyms:C₄₈H₃₀N₂O

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Chemical Property of C₄₈H₃₀N₂O

Chemical Property:

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Technology Process of C₄₈H₃₀N₂O

There total 5 articles about C₄₈H₃₀N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 86-76-0
2-bromodibenzo[b,d]furan

: 1428635-17-9
C₃₆H₂₄N₂

: 1428635-33-9
C₄₈H₃₀N₂O

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In 5,5-dimethyl-1,3-cyclohexadiene; for 20h; Inert atmosphere; Reflux;

Reference yield:

: 854952-58-2
N-phenyl-9H-carbazol-3-boronic acid

: 1428635-33-9
C₄₈H₃₀N₂O

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene; 1,2-dimethoxyethane; water / 15 h / Inert atmosphere; Reflux

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 8 h / Inert atmosphere; Reflux

3: palladium diacetate; tricyclohexylphosphine tetrafluoroborate; potassium carbonate / N,N-dimethyl acetamide / 15 h / 130 °C / Inert atmosphere

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate / 5,5-dimethyl-1,3-cyclohexadiene / 20 h / Inert atmosphere; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; sodium carbonate; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tricyclohexylphosphine tetrafluoroborate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In 1,2-dimethoxyethane; 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl acetamide; water; toluene;

Reference yield:

: 1428635-15-7
C₃₆H₂₅ClN₂

: 1428635-33-9
C₄₈H₃₀N₂O

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; tricyclohexylphosphine tetrafluoroborate; potassium carbonate / N,N-dimethyl acetamide / 15 h / 130 °C / Inert atmosphere

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate / 5,5-dimethyl-1,3-cyclohexadiene / 20 h / Inert atmosphere; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl acetamide;