Technology Process of C13H16O2
There total 5 articles about C13H16O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / diethyl ether; mineral oil / 1 h / 20 °C / Inert atmosphere
1.2: 16 h / 40 °C / Inert atmosphere
2.1: chloroform / 0.5 h / 20 °C / Inert atmosphere
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C
4.1: sodium periodate; hydrogenchloride / water; tetrahydrofuran / 2 h / 20 °C
With
hydrogenchloride; sodium periodate; sodium hydride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; diethyl ether; dichloromethane; chloroform; water; mineral oil;
DOI:10.1021/ja3116795
- Guidance literature:
-
With
hydrogenchloride; sodium periodate;
In
tetrahydrofuran; water;
at 20 ℃;
for 2h;
DOI:10.1021/ja3116795
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / diethyl ether; mineral oil / 1 h / 20 °C / Inert atmosphere
1.2: 16 h / 40 °C / Inert atmosphere
2.1: chloroform / 0.5 h / 20 °C / Inert atmosphere
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C
4.1: sodium periodate; hydrogenchloride / water; tetrahydrofuran / 2 h / 20 °C
With
hydrogenchloride; sodium periodate; sodium hydride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; diethyl ether; dichloromethane; chloroform; water; mineral oil;
DOI:10.1021/ja3116795