[(η2-Ph2PCH2CH2PPh2)(η5-C5Me5)Fe(CO)][PF6]

Base Information

Chemical Name:[(η2-Ph2PCH2CH2PPh2)(η5-C5Me5)Fe(CO)][PF6]
CAS No.:88251-02-9
Molecular Formula:C₃₇H₃₉FeOP₂*F₆P
Molecular Weight:762.475
Hs Code.:

Synonyms:[(η2-Ph2PCH2CH2PPh2)(η5-C5Me5)Fe(CO)][PF6]

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Chemical Property of [(η2-Ph2PCH2CH2PPh2)(η5-C5Me5)Fe(CO)][PF6]

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Technology Process of [(η2-Ph2PCH2CH2PPh2)(η5-C5Me5)Fe(CO)][PF6]

There total 4 articles about [(η2-Ph2PCH2CH2PPh2)(η5-C5Me5)Fe(CO)][PF6] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 17084-13-8
potassium hexafluorophosphate

: [Fe(pentamethylcyclopentadienyl)(CO)₂Cl]

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 88251-02-9
[(η2-Ph2PCH2CH2PPh2)(η5-C5Me5)Fe(CO)][PF6]

Guidance literature:: In toluene; Irradiation (UV/VIS); (Ar) soln. Fe complex in toluene was irradiated overnight with Heraeus UV lamp (150 W) , ppt. was filtered, washed with toluene, suspended in THF and KPF6 was added, stirred for 1 h; solvent was evapd., residue was extd. with CH2Cl2, evapd. to dryness, washed with Et2O and n-pentane and dried in vacuo;
DOI:10.1021/om100665u

Reference yield: 90.0%

: 86991-96-0
Fe(C₅(CH₃)5)(((C₆H₅)2PCH₂)2)(NCCH₃)⁽¹⁺⁾*PF₆^(1-)*99C₄H₈O

: 88251-02-9
[(η2-Ph2PCH2CH2PPh2)(η5-C5Me5)Fe(CO)][PF6]

Guidance literature:: With CO; In 1,2-dichloro-ethane; The soln. was stirred at 60°C under 3 atm of CO for 12 h;; concd. in vac., Et2O was added; recrystd. from acetone-ethanol; elem. anal.;;
DOI:10.1021/om00085a022