1-benzylimino-6-methyl-9-carbomethoxymethyl-1,2,3,4-tetrahydrocarbazole

Base Information

Chemical Name:1-benzylimino-6-methyl-9-carbomethoxymethyl-1,2,3,4-tetrahydrocarbazole
CAS No.:115174-32-8
Molecular Formula:C₂₃H₂₄N₂O₂
Molecular Weight:360.456
Hs Code.:

Synonyms:1-benzylimino-6-methyl-9-carbomethoxymethyl-1,2,3,4-tetrahydrocarbazole

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Chemical Property of 1-benzylimino-6-methyl-9-carbomethoxymethyl-1,2,3,4-tetrahydrocarbazole

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Technology Process of 1-benzylimino-6-methyl-9-carbomethoxymethyl-1,2,3,4-tetrahydrocarbazole

There total 3 articles about 1-benzylimino-6-methyl-9-carbomethoxymethyl-1,2,3,4-tetrahydrocarbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 115174-30-6
1-benzylimino-6-methyl-1,2,3,4-tetrahydrocarbazole

: 96-32-2
bromoacetic acid methyl ester

: 115174-32-8
1-benzylimino-6-methyl-9-carbomethoxymethyl-1,2,3,4-tetrahydrocarbazole

Guidance literature:: With sodium hydroxide; In water; benzene; at 25 ℃; for 1h; phase transfer with tetrabutylammonium bromide;
DOI:10.1007/BF00472254

Reference yield:

: 3449-48-7,812649-03-9
6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one

: 115174-32-8
1-benzylimino-6-methyl-9-carbomethoxymethyl-1,2,3,4-tetrahydrocarbazole

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / xylene / 3 h / Heating

2: 78 percent / NaOH / H₂O; benzene / 1 h / 25 °C / phase transfer with tetrabutylammonium bromide

With sodium hydroxide; In water; xylene; benzene;
DOI:10.1007/BF00472254

Reference yield:

: 100-46-9
benzylamine

: 115174-32-8
1-benzylimino-6-methyl-9-carbomethoxymethyl-1,2,3,4-tetrahydrocarbazole

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / xylene / 3 h / Heating

2: 78 percent / NaOH / H₂O; benzene / 1 h / 25 °C / phase transfer with tetrabutylammonium bromide

With sodium hydroxide; In water; xylene; benzene;
DOI:10.1007/BF00472254