2-(hydroxymethyl)-N-phenylacrylamide

Base Information

Chemical Name:2-(hydroxymethyl)-N-phenylacrylamide
CAS No.:442900-08-5
Molecular Formula:C₁₀H₁₁NO₂
Molecular Weight:177.203
Hs Code.:

Synonyms:2-(hydroxymethyl)-N-phenylacrylamide

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Chemical Property of 2-(hydroxymethyl)-N-phenylacrylamide

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Technology Process of 2-(hydroxymethyl)-N-phenylacrylamide

There total 6 articles about 2-(hydroxymethyl)-N-phenylacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 17408-14-9
1-(2-(trifluoromethyl)phenyl)ethan-1-one

: 2-((5,5-dimethyl-1,3,2-dioxaborinan-2-yl)methyl)-N-phenylacrylamide

: 442900-08-5
2-(hydroxymethyl)-N-phenylacrylamide

: (S)-4-hydroxy-2-methylene-N-phenyl-4-(2-(trifluoromethyl)phenyl)pentanamide

Guidance literature:: With water; (S)-2-(((1-(didecylamino)-3-methylbutan-2-yl)amino)methyl)phenol; zinc(II) hydroxide; In neat (no solvent); at 20 ℃; for 24h; Solvent; Reagent/catalyst; enantioselective reaction; Catalytic behavior; Green chemistry;
DOI:10.1002/adsc.202000195

Reference yield: 72.0%

: 1611-83-2
2-methyl-N-phenylacrylamide

: 442900-08-5
2-(hydroxymethyl)-N-phenylacrylamide

Guidance literature:: 2-methyl-N-phenylacrylamide; With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h; Inert atmosphere;

With Trimethyl borate; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; hexane; water; at 20 ℃; for 9h; Inert atmosphere;
DOI:10.1002/ejoc.201800084

Reference yield: 22.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 2210-24-4
N-acryloylaniline

: 442900-08-5
2-(hydroxymethyl)-N-phenylacrylamide

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In water; tert-butyl alcohol; phenol; at 55 ℃; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.jmedchem.0c00749