trans-1-phenyl-4-tert-butylcyclohexanecarboxylic acid

Base Information

Chemical Name:trans-1-phenyl-4-tert-butylcyclohexanecarboxylic acid
CAS No.:53517-40-1
Molecular Formula:C₁₇H₂₄O₂
Molecular Weight:260.376
Hs Code.:

Synonyms:trans-1-phenyl-4-tert-butylcyclohexanecarboxylic acid

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Chemical Property of trans-1-phenyl-4-tert-butylcyclohexanecarboxylic acid

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Technology Process of trans-1-phenyl-4-tert-butylcyclohexanecarboxylic acid

There total 3 articles about trans-1-phenyl-4-tert-butylcyclohexanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 52866-66-7
cis-methyl 1-phenyl-4-tert-butylcyclohexanecarboxylate

: 53517-40-1
trans-1-phenyl-4-tert-butylcyclohexanecarboxylic acid

Guidance literature:: With potassium hydroxide; In ethanol; for 3h; Heating;
DOI:10.1021/jo00256a014

Reference yield:

: 758-75-8
1-bromo-3-(2-bromoethyl)-4,4-dimethylpentane

: 53517-40-1
trans-1-phenyl-4-tert-butylcyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / NaI, NaH, hexamethylphosphoramide / dimethylformamide / 2 h / 0 °C

2: 100 percent / 20percent aq. KOH / ethanol / 3 h / Heating

With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hydroxide; sodium hydride; sodium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00256a014

Reference yield:

: 101-41-7
benzeneacetic acid methyl ester

: 53517-40-1
trans-1-phenyl-4-tert-butylcyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / NaI, NaH, hexamethylphosphoramide / dimethylformamide / 2 h / 0 °C

2: 100 percent / 20percent aq. KOH / ethanol / 3 h / Heating

With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hydroxide; sodium hydride; sodium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00256a014