trans-1-benzoyl-1-phenyl-4-tert-butylcyclohexane

Base Information

Chemical Name:trans-1-benzoyl-1-phenyl-4-tert-butylcyclohexane
CAS No.:116350-19-7
Molecular Formula:C₂₃H₂₈O
Molecular Weight:320.475
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-1-benzoyl-1-phenyl-4-tert-butylcyclohexane

Chemical Property:

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Technology Process of trans-1-benzoyl-1-phenyl-4-tert-butylcyclohexane

There total 5 articles about trans-1-benzoyl-1-phenyl-4-tert-butylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 591-51-5
phenyllithium

: 53517-42-3
4-tert-Butyl-1-phenyl-cyclohexanecarbonyl chloride

: 116350-19-7
trans-1-benzoyl-1-phenyl-4-tert-butylcyclohexane

Guidance literature:: With iron(III)-acetylacetonate; In diethyl ether; cyclohexane; at 0 ℃; for 0.5h; Yield given;
DOI:10.1021/jo00256a014

Reference yield:

: 758-75-8
1-bromo-3-(2-bromoethyl)-4,4-dimethylpentane

: 116350-19-7
trans-1-benzoyl-1-phenyl-4-tert-butylcyclohexane

Guidance literature:: Multi-step reaction with 4 steps

1: 41 percent / NaI, NaH, hexamethylphosphoramide / dimethylformamide / 2 h / 0 °C

2: 100 percent / 20percent aq. KOH / ethanol / 3 h / Heating

3: thionyl chloride / benzene / 2 h / Heating

4: Fe(acac)3 / diethyl ether; cyclohexane / 0.5 h / 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hydroxide; thionyl chloride; iron(III)-acetylacetonate; sodium hydride; sodium iodide; In diethyl ether; ethanol; cyclohexane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00256a014

Reference yield:

: 53517-40-1
trans-1-phenyl-4-tert-butylcyclohexanecarboxylic acid

: 116350-19-7
trans-1-benzoyl-1-phenyl-4-tert-butylcyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / benzene / 2 h / Heating

2: Fe(acac)3 / diethyl ether; cyclohexane / 0.5 h / 0 °C

With thionyl chloride; iron(III)-acetylacetonate; In diethyl ether; cyclohexane; benzene;
DOI:10.1021/jo00256a014