5-[(4S,5S)-5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl]-(2R)-(trifluoroacetyl)amino-4-(Z)-pentenoic acid tert-butyl ester

Base Information

Chemical Name:5-[(4S,5S)-5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl]-(2R)-(trifluoroacetyl)amino-4-(Z)-pentenoic acid tert-butyl ester
CAS No.:1108179-39-0
Molecular Formula:C₂₄H₃₂F₃NO₆
Molecular Weight:487.516
Hs Code.:

Synonyms:5-[(4S,5S)-5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl]-(2R)-(trifluoroacetyl)amino-4-(Z)-pentenoic acid tert-butyl ester

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Chemical Property of 5-[(4S,5S)-5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl]-(2R)-(trifluoroacetyl)amino-4-(Z)-pentenoic acid tert-butyl ester

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Technology Process of 5-[(4S,5S)-5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl]-(2R)-(trifluoroacetyl)amino-4-(Z)-pentenoic acid tert-butyl ester

There total 1 articles about 5-[(4S,5S)-5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl]-(2R)-(trifluoroacetyl)amino-4-(Z)-pentenoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1108179-32-3
(Z)-3-((4S,5S)-5-benzyloxymethyl-2,2-dimethyl-[1,3]-dioxolan-4-yl)-allyl diethyl phosphate

: 63959-88-6
tert-butyl N-(trifluoroacetyl)glycinate

: 1108179-39-0
5-[(4S,5S)-5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl]-(2R)-(trifluoroacetyl)amino-4-(Z)-pentenoic acid tert-butyl ester

Guidance literature:: tert-butyl N-(trifluoroacetyl)glycinate; With zinc(II) chloride; lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.333333h;

(Z)-3-((4S,5S)-5-benzyloxymethyl-2,2-dimethyl-[1,3]-dioxolan-4-yl)-allyl diethyl phosphate; With bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine; In tetrahydrofuran; at -78 - 20 ℃; optical yield given as %de; stereoselective reaction;
DOI:10.1039/b813978d