dimethyl (3R,4R,5S)-4-azido-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

Base Information

Chemical Name:dimethyl (3R,4R,5S)-4-azido-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate
CAS No.:945621-37-4
Molecular Formula:C₁₂H₂₂N₃O₇P
Molecular Weight:351.296
Hs Code.:

Synonyms:dimethyl (3R,4R,5S)-4-azido-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

Suppliers and Price of dimethyl (3R,4R,5S)-4-azido-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dimethyl (3R,4R,5S)-4-azido-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dimethyl (3R,4R,5S)-4-azido-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

There total 3 articles about dimethyl (3R,4R,5S)-4-azido-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1065011-17-7
C₁₃H₂₂O₁₀PSF₃

: 945621-37-4
dimethyl (3R,4R,5S)-4-azido-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

Guidance literature:: With sodium azide; tert-butylamine hydrochloride; In N,N-dimethyl-formamide; at 50 ℃;
DOI:10.1080/07328300701351532

Reference yield:

: 945621-35-2
dimethyl (3R,4S,5S)-4-benzyloxy-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

: 945621-37-4
dimethyl (3R,4R,5S)-4-azido-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / 1,4-cyclohexadiene / Pearlman's catalyst / ethanol / 96 h / 50 °C

2: pyridine / CH₂Cl₂ / 2 h / -10 °C

3: 86 percent / NaN₃; tert-butylamine hydrochloride / dimethylformamide / 50 °C

With pyridine; sodium azide; cyclohexa-1,4-diene; tert-butylamine hydrochloride; palladium dihydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/07328300701351532

Reference yield:

: 945621-36-3
dimethyl (3R,4S,5S)-4-hydroxy-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

: 945621-37-4
dimethyl (3R,4R,5S)-4-azido-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 2 h / -10 °C

2: 86 percent / NaN₃; tert-butylamine hydrochloride / dimethylformamide / 50 °C

With pyridine; sodium azide; tert-butylamine hydrochloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/07328300701351532