dimethyl (3R,4S,5S)-4-hydroxy-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

Base Information

Chemical Name:dimethyl (3R,4S,5S)-4-hydroxy-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate
CAS No.:945621-36-3
Molecular Formula:C₁₂H₂₃O₈P
Molecular Weight:326.284
Hs Code.:

Synonyms:dimethyl (3R,4S,5S)-4-hydroxy-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl (3R,4S,5S)-4-hydroxy-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

Chemical Property:

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Technology Process of dimethyl (3R,4S,5S)-4-hydroxy-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

There total 1 articles about dimethyl (3R,4S,5S)-4-hydroxy-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 945621-35-2
dimethyl (3R,4S,5S)-4-benzyloxy-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

: 945621-36-3
dimethyl (3R,4S,5S)-4-hydroxy-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

Guidance literature:: With cyclohexa-1,4-diene; palladium dihydroxide; In ethanol; at 50 ℃; for 96h;
DOI:10.1080/07328300701351532

Reference yield:

: 945621-36-3
dimethyl (3R,4S,5S)-4-hydroxy-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

: 358-23-6
trifluoromethylsulfonic anhydride

: 1065011-17-7
C₁₃H₂₂O₁₀PSF₃

Guidance literature:: With pyridine; In dichloromethane; at -10 ℃; for 2h;
DOI:10.1080/07328300701351532

Reference yield:

: 945621-36-3
dimethyl (3R,4S,5S)-4-hydroxy-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

: 945621-37-4
dimethyl (3R,4R,5S)-4-azido-3,5-di(methoxymethyloxy)-1-cyclohexenephosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 2 h / -10 °C

2: 86 percent / NaN₃; tert-butylamine hydrochloride / dimethylformamide / 50 °C

With pyridine; sodium azide; tert-butylamine hydrochloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/07328300701351532