bis(triphenylphosphine)(4,5,9,14-tetraaza-benzo[b]triphenylene)copper(I) tetrafluoroborate

Base Information

Chemical Name:bis(triphenylphosphine)(4,5,9,14-tetraaza-benzo[b]triphenylene)copper(I) tetrafluoroborate
CAS No.:205367-18-6
Molecular Formula:BF₄*C₅₄H₄₀CuN₄P₂
Molecular Weight:957.237
Hs Code.:

Synonyms:bis(triphenylphosphine)(4,5,9,14-tetraaza-benzo[b]triphenylene)copper(I) tetrafluoroborate

Suppliers and Price of bis(triphenylphosphine)(4,5,9,14-tetraaza-benzo[b]triphenylene)copper(I) tetrafluoroborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(triphenylphosphine)(4,5,9,14-tetraaza-benzo[b]triphenylene)copper(I) tetrafluoroborate

Chemical Property:

Purity/Quality:

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Technology Process of bis(triphenylphosphine)(4,5,9,14-tetraaza-benzo[b]triphenylene)copper(I) tetrafluoroborate

There total 4 articles about bis(triphenylphosphine)(4,5,9,14-tetraaza-benzo[b]triphenylene)copper(I) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 19535-47-8
dipyridil[3,2-a:2',3'-c]phenazine

: 114074-99-6
[copper(I)(acetonitrile)2(PPh3)2](BF4)

: 205367-18-6
bis(triphenylphosphine)(4,5,9,14-tetraaza-benzo[b]triphenylene)copper(I) tetrafluoroborate

Guidance literature:: In dichloromethane; (argon); rapid reaction at room temp.; recrystn. (MeOH); elem. anal.;
DOI:10.1039/a706110b

Reference yield:

: 19535-47-8
dipyridil[3,2-a:2',3'-c]phenazine

: tetrakis(acetonitrile)copper(I)tetrafluoroborate

: 603-35-0
triphenylphosphine

: 205367-18-6
bis(triphenylphosphine)(4,5,9,14-tetraaza-benzo[b]triphenylene)copper(I) tetrafluoroborate

Guidance literature:: tetrakis(acetonitrile)copper(I)tetrafluoroborate; triphenylphosphine; In dichloromethane; at 20 ℃; for 0.5h;

dipyridil[3,2-a:2',3'-c]phenazine; In vaseline; for 1h;
DOI:10.1016/j.saa.2012.11.044

Reference yield:

: 66-71-7
1,10-Phenanthroline

: 205367-18-6
bis(triphenylphosphine)(4,5,9,14-tetraaza-benzo[b]triphenylene)copper(I) tetrafluoroborate

Guidance literature:: Multi-step reaction with 3 steps

1.1: nitric acid; sulfuric acid; potassium bromide

2.1: ethanol / 10 h / Heating

3.1: dichloromethane / 0.5 h

3.2: 0.5 h

With sulfuric acid; nitric acid; potassium bromide; In ethanol; dichloromethane;
DOI:10.1016/j.saa.2020.118537