C₄₀H₅₃NO₅

Base Information

Chemical Name:C₄₀H₅₃NO₅
CAS No.:1213270-07-5
Molecular Formula:C₄₀H₅₃NO₅
Molecular Weight:627.865
Hs Code.:

C<sub>40</sub>H<sub>53</sub>NO<sub>5</sub>

Synonyms:C₄₀H₅₃NO₅

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Chemical Property of C₄₀H₅₃NO₅

Chemical Property:

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Technology Process of C₄₀H₅₃NO₅

There total 10 articles about C₄₀H₅₃NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1213270-06-4
C₂₀H₃₀BNO₄

: 1213270-05-3
C₂₆H₃₅BrO₃

: 1213270-07-5
C₄₀H₅₃NO₅

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium hydroxide; In water; toluene; at 90 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol100214X

Reference yield:

: 1213270-03-1
C₂₁H₂₉BrO₂

: 1213270-07-5
C₄₀H₅₃NO₅

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; triethylamine / dichloromethane / 0.33 h / 0 - 23 °C / Inert atmosphere

2: bromine; sodium acetate; acetic acid / 4 h / 60 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydroxide / water; toluene / 0.92 h / 90 °C / Inert atmosphere

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium hydroxide / water; toluene / 0.5 h / 90 °C / Inert atmosphere

With dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; bromine; sodium acetate; acetic acid; triethylamine; sodium hydroxide; In dichloromethane; water; toluene; 3: Suzuki coupling / 4: Suzuki coupling;
DOI:10.1039/c1ob06363d

Reference yield:

: 1213270-13-3
C₂₃H₃₁BrO₃

: 1213270-07-5
C₄₀H₅₃NO₅

Guidance literature:: Multi-step reaction with 3 steps

1: bromine; sodium acetate; acetic acid / 4 h / 60 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydroxide / water; toluene / 0.92 h / 90 °C / Inert atmosphere

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium hydroxide / water; toluene / 0.5 h / 90 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; bromine; sodium acetate; acetic acid; sodium hydroxide; In water; toluene; 2: Suzuki coupling / 3: Suzuki coupling;
DOI:10.1039/c1ob06363d